1,2-bisethane

Base Information

Chemical Name:1,2-bisethane
CAS No.:98815-25-9
Molecular Formula:C₃₄H₄₄N₄P₂
Molecular Weight:570.698
Hs Code.:

1,2-bis<bis(p-dimethylaminophenyl)phosphino>ethane

Synonyms:

Suppliers and Price of 1,2-bisethane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,2-bisethane

Chemical Property:

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Technology Process of 1,2-bisethane

There total 1 articles about 1,2-bisethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 28240-69-9
1,2-bis(dichlorophosphino)ethane

: 586-77-6
4-bromo-N,N-dimethylaniline

: 98815-25-9
1,2-bisethane

Guidance literature:: With n-butyllithium; Yield given. Multistep reaction; 1) hexane, Et₂O, RT, 15 min; 2) hexane, Et₂O, RT, 12 h;
DOI:10.1039/DT9850001131

Reference yield: 84.0%

: di(rhodium)tetracarbonyl dichloride

: 98815-25-9
1,2-bisethane

: 1189131-82-5
cis-[Rh(CO)Cl(bis-1,2(di(4-dimethylaminophenyl)phosphino)ethane)]

Guidance literature:: In tetrahydrofuran; N2; THF soln. of ligand (0.154 mmol) added dropwise to THF soln. of Rh compd. (0.077 mmol), mixt. stirred for 4 h; pptd., filtered off (under Ar), washed (cold pentane), elem. anal.;
DOI:10.1016/j.ica.2009.05.064

Reference yield:

: 98815-25-9
1,2-bisethane

: [Rh(COCH₃)I₂(bis-1,2(di(4-dimethylaminophenyl)phosphino)ethane)]

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran

2: acetic acid methyl ester

In tetrahydrofuran; acetic acid methyl ester;
DOI:10.1016/j.ica.2009.05.064