Technology Process of C38H49ClO13Si
There total 7 articles about C38H49ClO13Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 73 percent / DMAP / CH2Cl2 / 15 h / Ambient temperature
2: 87 percent / NaBH4 / ethanol; CH2Cl2 / 5 h / 0 °C
3: 67 percent / POCl3, pyridine / 4 h / 100 °C
With
pyridine; dmap; sodium tetrahydroborate; trichlorophosphate;
In
ethanol; dichloromethane;
DOI:10.1021/jo00289a027
- Guidance literature:
-
Multi-step reaction with 6 steps
1: DMAP, pyridine / 0 deg C, 1h, warming up to RT
2: tributyltin hydride, AIBN / toluene / 2 h / Heating
3: 73 percent / DMAP / CH2Cl2 / 15 h / Ambient temperature
4: 87 percent / NaBH4 / ethanol; CH2Cl2 / 5 h / 0 °C
5: 67 percent / POCl3, pyridine / 4 h / 100 °C
With
pyridine; dmap; sodium tetrahydroborate; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; trichlorophosphate;
In
ethanol; dichloromethane; toluene;
DOI:10.1021/jo00289a027
- Guidance literature:
-
Multi-step reaction with 5 steps
1: tributyltin hydride, AIBN / toluene / 2 h / Heating
2: 73 percent / DMAP / CH2Cl2 / 15 h / Ambient temperature
3: 87 percent / NaBH4 / ethanol; CH2Cl2 / 5 h / 0 °C
4: 67 percent / POCl3, pyridine / 4 h / 100 °C
With
pyridine; dmap; sodium tetrahydroborate; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; trichlorophosphate;
In
ethanol; dichloromethane; toluene;
DOI:10.1021/jo00289a027
