methyl onate

Base Information

Chemical Name:methyl onate
CAS No.:131156-51-9
Molecular Formula:C₃₂H₆₆O₇Si₃
Molecular Weight:647.128
Hs Code.:

methyl <cyclohexyl 4,5,7-tri-O-(t-butyldimethylsilyl)-2-deoxy-αβ-D-lyxo-2-heptulopyranosid>onate

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Suppliers and Price of methyl onate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl onate

Chemical Property:

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Technology Process of methyl onate

There total 8 articles about methyl onate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 125211-47-4,125211-48-5
methyl onate

: 108-93-0
cyclohexanol

: 125211-53-2
1-methoxycarbonyl-3,4,6-tri-O-(t-butyldimethylsilyl)-D-galactal

: 131156-51-9
methyl onate

Guidance literature:: With N-Bromosuccinimide; molecular sieve; In dichloromethane; for 3h; Ambient temperature;

Reference yield: 29.0%

: 125211-47-4,125211-48-5
methyl onate

: 125211-53-2
1-methoxycarbonyl-3,4,6-tri-O-(t-butyldimethylsilyl)-D-galactal

: 131156-51-9
methyl onate

Guidance literature:: With N-Bromosuccinimide; molecular sieve; cyclohexanol; In dichloromethane; for 3h; Ambient temperature;

Reference yield:

: 121702-69-0
(((2R,3S,4R)-2-(((tert-butyldimethylsilyl)oxy)methyl)-3,4-dihydro-2H-pyran-3,4-diyl)bis(oxy))bis(tert-butyldimethylsilane)

: 131156-51-9
methyl onate

Guidance literature:: Multi-step reaction with 4 steps

1: 1) HCl, 2) iPr₂NEt / 1) toluene, 0 deg C, 10 min, 2) CH₂Cl₂, r.t., 1.5h; or with catalyst camphor-10-sulphonic acid

2: 96 percent / magnesium monoperoxyphthalate / ethanol / Ambient temperature

4: 29 percent / cyclohexanol, NBS, molecular sieves / CH₂Cl₂ / 3 h / Ambient temperature

With hydrogenchloride; N-Bromosuccinimide; molecular sieve; magnesium monoperoxyphthalate hexahydrate; N-ethyl-N,N-diisopropylamine; cyclohexanol; In ethanol; dichloromethane;