2,4-dibenzoyl-1-methyl-benzene

Base Information

• Chemical Name: 2,4-dibenzoyl-1-methyl-benzene
• CAS No.: 859794-05-1
• Molecular Formula: C₂₁H₁₆O₂
• Molecular Weight: 300.357
• Mol file: 859794-05-1.mol

Synonyms:

Chemical Property of 2,4-dibenzoyl-1-methyl-benzene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,4-dibenzoyl-1-methyl-benzene

There total 7 articles about 2,4-dibenzoyl-1-methyl-benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-benzoyl-2-methyl-benzoic acid (321879-70-3) → 2,4-dibenzoyl-1-methyl-benzene (859794-05-1)

Guidance literature:

With phosphorus pentachloride; benzene; Behandeln des Reaktionsprodukts mit Benzol und AlCl₃ bei 60grad;

Reference yield:

4-Methylbenzophenone (134-84-9) → 2,4-dibenzoyl-1-methyl-benzene (859794-05-1)

Guidance literature:

Multi-step reaction with 5 steps

1: aqueous HNO₃ / 80 °C

2: sodium sulfide; aqueous ethanol

3: aqueous hydrochloric acid; sodium nitrite / Diazotization_.Erwaermen einer Diazoniumsalz-Loesung mit einer aus Kaliumcyanid, Kupfer(II)-sulfat und Wasser hergestellten Loesung

4: aqueous sulfuric acid

5: PCl₅; benzene / Behandeln des Reaktionsprodukts mit Benzol und AlCl₃ bei 60grad

With hydrogenchloride; sodium sulfide; ethanol; phosphorus pentachloride; sulfuric acid; nitric acid; sodium nitrite; benzene;

Reference yield:

4-methyl-3-nitrobenzophenone (79482-00-1) → 2,4-dibenzoyl-1-methyl-benzene (859794-05-1)

Guidance literature:

Multi-step reaction with 4 steps

1: sodium sulfide; aqueous ethanol

2: aqueous hydrochloric acid; sodium nitrite / Diazotization_.Erwaermen einer Diazoniumsalz-Loesung mit einer aus Kaliumcyanid, Kupfer(II)-sulfat und Wasser hergestellten Loesung

3: aqueous sulfuric acid

4: PCl₅; benzene / Behandeln des Reaktionsprodukts mit Benzol und AlCl₃ bei 60grad

With hydrogenchloride; sodium sulfide; ethanol; phosphorus pentachloride; sulfuric acid; sodium nitrite; benzene;

upstream raw materials:

5-benzoyl-2-methyl-benzoic acid

4-Methylbenzophenone

4-methyl-3-nitrobenzophenone

3-amino-4-methyl-benzophenone

Downstream raw materials:

2-benzoylanthracene-9,10-dione

2,4-dibenzoyl-benzoic acid