Technology Process of C40H58O6SSi2
There total 34 articles about C40H58O6SSi2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 8 steps
2: ZnBr2 / CH2Cl2
3: 11 percent / TsOH / benzene
4: 90 percent / 2,6-lutidine / CH2Cl2
5: L-Selectride / tetrahydrofuran / -78 °C
6: 2,6-lutidine
7: 1.) LDA, HMPA, 2.) PhSe(O)Cl / 1.) THF, 0 deg C
8: Cs2CO3 / 0 °C
With
2,6-dimethylpyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; benzeneseleninyl chloride; L-Selectride; caesium carbonate; toluene-4-sulfonic acid; zinc dibromide; lithium diisopropyl amide;
In
tetrahydrofuran; dichloromethane; benzene;
- Guidance literature:
-
Multi-step reaction with 8 steps
2: ZnBr2 / CH2Cl2
3: 11 percent / TsOH / benzene
4: 90 percent / 2,6-lutidine / CH2Cl2
5: L-Selectride / tetrahydrofuran / -78 °C
6: 2,6-lutidine
7: 1.) LDA, HMPA, 2.) PhSe(O)Cl / 1.) THF, 0 deg C
8: Cs2CO3 / 0 °C
With
2,6-dimethylpyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; benzeneseleninyl chloride; L-Selectride; caesium carbonate; toluene-4-sulfonic acid; zinc dibromide; lithium diisopropyl amide;
In
tetrahydrofuran; dichloromethane; benzene;
- Guidance literature:
-
Multi-step reaction with 11 steps
1: 1.) BH3, 2.) NaOH, H2O2 / 1.) THF, 2.) 0 deg C
2: 2,6-lutidine / CH2Cl2
3: DIBAL-H / toluene / -78 °C
5: ZnBr2 / CH2Cl2
6: 11 percent / TsOH / benzene
7: 90 percent / 2,6-lutidine / CH2Cl2
8: L-Selectride / tetrahydrofuran / -78 °C
9: 2,6-lutidine
10: 1.) LDA, HMPA, 2.) PhSe(O)Cl / 1.) THF, 0 deg C
11: Cs2CO3 / 0 °C
With
2,6-dimethylpyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; sodium hydroxide; benzeneseleninyl chloride; borane; dihydrogen peroxide; L-Selectride; diisobutylaluminium hydride; caesium carbonate; toluene-4-sulfonic acid; zinc dibromide; lithium diisopropyl amide;
In
tetrahydrofuran; dichloromethane; toluene; benzene;