Technology Process of (E,E)-1,8-bisphenylsulphonylocta-1,7-diene
There total 8 articles about (E,E)-1,8-bisphenylsulphonylocta-1,7-diene which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 1) tBuOCl / 1) r.t., 1 h, ethyl acetate, 2) ethyl acetate
2: 97 percent / H2 / 10percent Pd-C / ethyl acetate
3: 50 percent / 100 °C / 20 Torr
4: 30 percent / light petroleum / 69 h / 160 - 170 °C / 4-t-butylpyrocatechol
5: 1) CH2Cl2, 2) DMSO, 100 deg C, 1,5 h
6: 2.44 g / 85percent mCPBA / CH2Cl2 / 1 h / Ambient temperature
7: 2.82 g / NaOAc / dimethylsulfoxide / 2 h / Ambient temperature
With
tert-butylhypochlorite; hydrogen; sodium acetate; 3-chloro-benzenecarboperoxoic acid;
palladium on activated charcoal;
In
dichloromethane; dimethyl sulfoxide; ethyl acetate; Petroleum ether;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 97 percent / H2 / 10percent Pd-C / ethyl acetate
2: 50 percent / 100 °C / 20 Torr
3: 30 percent / light petroleum / 69 h / 160 - 170 °C / 4-t-butylpyrocatechol
4: 1) CH2Cl2, 2) DMSO, 100 deg C, 1,5 h
5: 2.44 g / 85percent mCPBA / CH2Cl2 / 1 h / Ambient temperature
6: 2.82 g / NaOAc / dimethylsulfoxide / 2 h / Ambient temperature
With
hydrogen; sodium acetate; 3-chloro-benzenecarboperoxoic acid;
palladium on activated charcoal;
In
dichloromethane; dimethyl sulfoxide; ethyl acetate; Petroleum ether;
- Guidance literature:
-
With
sodium acetate;
In
dimethyl sulfoxide;
for 2h;
Ambient temperature;
