Technology Process of C34H40N2O15
There total 10 articles about C34H40N2O15 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
carbon tetrabromide;
In
isopropyl alcohol;
for 4h;
Reflux;
Inert atmosphere;
DOI:10.1021/ja4108676
- Guidance literature:
-
Multi-step reaction with 5 steps
1: bis-triphenylphosphine-palladium(II) chloride / toluene / 48 h / Reflux
2: lithium aluminium tetrahydride / tetrahydrofuran / 12 h / 0 - 20 °C
3: potassium carbonate; 18-crown-6 ether / acetone / 12 h / Reflux
4: potassium carbonate; 18-crown-6 ether / acetone / 12 h / Reflux; Inert atmosphere
5: carbon tetrabromide / isopropyl alcohol / 4 h / Reflux; Inert atmosphere
With
bis-triphenylphosphine-palladium(II) chloride; lithium aluminium tetrahydride; 18-crown-6 ether; carbon tetrabromide; potassium carbonate;
In
tetrahydrofuran; isopropyl alcohol; acetone; toluene;
DOI:10.1021/ja4108676
- Guidance literature:
-
Multi-step reaction with 4 steps
1: lithium aluminium tetrahydride / tetrahydrofuran / 12 h / 0 - 20 °C
2: potassium carbonate; 18-crown-6 ether / acetone / 12 h / Reflux
3: potassium carbonate; 18-crown-6 ether / acetone / 12 h / Reflux; Inert atmosphere
4: carbon tetrabromide / isopropyl alcohol / 4 h / Reflux; Inert atmosphere
With
lithium aluminium tetrahydride; 18-crown-6 ether; carbon tetrabromide; potassium carbonate;
In
tetrahydrofuran; isopropyl alcohol; acetone;
DOI:10.1021/ja4108676