tris(pentafluorophenyl)aluminum*tetrahydrofuran

Base Information

Chemical Name:tris(pentafluorophenyl)aluminum*tetrahydrofuran
CAS No.:168704-95-8
Molecular Formula:C₄H₈O*C₁₈AlF₁₅
Molecular Weight:600.263
Hs Code.:

Synonyms:

Suppliers and Price of tris(pentafluorophenyl)aluminum*tetrahydrofuran

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of tris(pentafluorophenyl)aluminum*tetrahydrofuran

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of tris(pentafluorophenyl)aluminum*tetrahydrofuran

There total 4 articles about tris(pentafluorophenyl)aluminum*tetrahydrofuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 1184-58-3
dimethylaluminum chloride

: 1076-44-4
pentafluorophenyl lithium

: 168704-95-8
tris(pentafluorophenyl)aluminum*tetrahydrofuran

Guidance literature:: In hexane; byproducts: AlMe3, LiCl; dry N2-atmosphere; slow addn. of equimolar amt. Me2AlCl to C6F5Li (-78°C), stirring (overnight, room temp.), filtering, evapn. (vac.), slow heating (up to 180°C, 1E-3 Pa); recrystn. (boiling THF); elem. anal.;
DOI:10.1021/ic00118a033

Reference yield:

: 109-99-9,24979-97-3,77392-70-2
tetrahydrofuran

: 1109-15-5
tris(pentafluorophenyl)borate

: 75-24-1
trimethylaluminum

: 168704-95-8
tris(pentafluorophenyl)aluminum*tetrahydrofuran

Guidance literature:: tris(pentafluorophenyl)borate; trimethylaluminum; In toluene; at 20 ℃; for 2h;

tetrahydrofuran;
DOI:10.1002/pola.28383

Reference yield:

: tris(pentafluorophenyl)aluminum*(toluene)0.5

: 168704-95-8
tris(pentafluorophenyl)aluminum*tetrahydrofuran

Guidance literature:: In tetrahydrofuran; hexane; (inert atm.); educt dissolving in THF, hexane layering on top of soln., standing (2-3 d); elem. anal.;
DOI:10.1016/S1381-1169(97)00277-X