2-(2,6-dichlorophenyl)-1-hydroxyethylidenebisphosphonic acid

Base Information

Chemical Name:2-(2,6-dichlorophenyl)-1-hydroxyethylidenebisphosphonic acid
CAS No.:87616-78-2
Molecular Formula:C₈H₁₀Cl₂O₇P₂
Molecular Weight:351.017
Hs Code.:

Synonyms:

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Chemical Property of 2-(2,6-dichlorophenyl)-1-hydroxyethylidenebisphosphonic acid

Chemical Property:

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Technology Process of 2-(2,6-dichlorophenyl)-1-hydroxyethylidenebisphosphonic acid

There total 4 articles about 2-(2,6-dichlorophenyl)-1-hydroxyethylidenebisphosphonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₃H₅₀Cl₂O₇P₂Si₅

: 87616-78-2
2-(2,6-dichlorophenyl)-1-hydroxyethylidenebisphosphonic acid

Guidance literature:: With methanol; In tetrahydrofuran; for 1h;
DOI:10.1021/jf401234s

Reference yield:

: 6575-24-2
2-(2,6-dichlorophenyl)acetic acid

: 87616-78-2
2-(2,6-dichlorophenyl)-1-hydroxyethylidenebisphosphonic acid

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride / 1 h / Reflux

2: tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

3: methanol / tetrahydrofuran / 1 h

With methanol; thionyl chloride; In tetrahydrofuran;
DOI:10.1021/jf401234s

Reference yield:

: 61875-53-4
2,6-dichlorophenylacetylchloride

: 87616-78-2
2-(2,6-dichlorophenyl)-1-hydroxyethylidenebisphosphonic acid

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

2: methanol / tetrahydrofuran / 1 h

With methanol; In tetrahydrofuran;
DOI:10.1021/jf401234s