C₄₁H₅₁Cl₂N₃O₉S

Base Information

• Chemical Name: C₄₁H₅₁Cl₂N₃O₉S
• CAS No.: 116073-78-0
• Molecular Formula: C₄₁H₅₁Cl₂N₃O₉S
• Molecular Weight: 832.843
• Mol file: 116073-78-0.mol

Synonyms:

Chemical Property of C₄₁H₅₁Cl₂N₃O₉S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₄₁H₅₁Cl₂N₃O₉S

There total 14 articles about C₄₁H₅₁Cl₂N₃O₉S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,3'-Iminodipropionitrile (111-94-4) → C41H51Cl2N3O9S (116073-78-0)

Guidance literature:

Multi-step reaction with 10 steps

1: 89 percent / pyridine / 10 deg C, 30 min, RT, 4 h

2: 95 percent / hydrochlorid acid / H₂O / 2 h / Heating

3: 91 percent / sodium borohydride, borontrifluoride diethylether / tetrahydrofuran / 2 h / Ambient temperature

4: 1.) sodium hydride / 1.) THF, RT, 10 min, 2.) 4.5 h

5: 1.) lithium aluminium hydride, sulphuric acid / 1.) THF, 0 deg C, 2.) THF, RT, 3 h

6: 27 percent / Et₃N / CH₂Cl₂; toluene / 24 h / Ambient temperature

7: 96 percent / borane-THF complex / tetrahydrofuran / 2 h / Heating

8: 84 percent / triethylamine / tetrahydrofuran / 2.5 h

9: potassium hydroxide / methanol / 0.5 h / Heating

10: thionyl chloride / 4 h / Heating

With pyridine; hydrogenchloride; potassium hydroxide; sodium tetrahydroborate; lithium aluminium tetrahydride; thionyl chloride; borane-THF; sulfuric acid; boron trifluoride diethyl etherate; sodium hydride; triethylamine; In tetrahydrofuran; methanol; dichloromethane; water; toluene;

Reference yield:

2-cyanoethyl ether (1656-48-0) → C41H51Cl2N3O9S (116073-78-0)

Guidance literature:

Multi-step reaction with 7 steps

1: 6M hydrochlorid acid / H₂O / 2 h / Heating

2: thionyl chloride / 3 h / Heating

3: 27 percent / Et₃N / CH₂Cl₂; toluene / 24 h / Ambient temperature

4: 96 percent / borane-THF complex / tetrahydrofuran / 2 h / Heating

5: 84 percent / triethylamine / tetrahydrofuran / 2.5 h

6: potassium hydroxide / methanol / 0.5 h / Heating

7: thionyl chloride / 4 h / Heating

With hydrogenchloride; potassium hydroxide; thionyl chloride; borane-THF; triethylamine; In tetrahydrofuran; methanol; dichloromethane; water; toluene;

Reference yield:

3-(2-carboxyethoxy)propionic acid (5961-83-1) → C41H51Cl2N3O9S (116073-78-0)

Guidance literature:

Multi-step reaction with 6 steps

1: thionyl chloride / 3 h / Heating

2: 27 percent / Et₃N / CH₂Cl₂; toluene / 24 h / Ambient temperature

3: 96 percent / borane-THF complex / tetrahydrofuran / 2 h / Heating

4: 84 percent / triethylamine / tetrahydrofuran / 2.5 h

5: potassium hydroxide / methanol / 0.5 h / Heating

6: thionyl chloride / 4 h / Heating

With potassium hydroxide; thionyl chloride; borane-THF; triethylamine; In tetrahydrofuran; methanol; dichloromethane; toluene;

upstream raw materials:

C₄₁H₅₃N₃O₁₁S

2-cyanoethyl ether

3,3'-Iminodipropionitrile

3-(2-carboxyethoxy)propionic acid

Downstream raw materials:

C₆₆H₉₄N₆O₁₄S₂

Refernces