threo-2-methyl 3-hydroxy 3-phenylpropanoic methyl ester

Base Information

Chemical Name:threo-2-methyl 3-hydroxy 3-phenylpropanoic methyl ester
CAS No.:14366-89-3
Molecular Formula:C₁₁H₁₄O₃
Molecular Weight:194.23
Hs Code.:

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Chemical Property of threo-2-methyl 3-hydroxy 3-phenylpropanoic methyl ester

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Technology Process of threo-2-methyl 3-hydroxy 3-phenylpropanoic methyl ester

There total 139 articles about threo-2-methyl 3-hydroxy 3-phenylpropanoic methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 89337-61-1
tert-butyl((1-methoxyprop-1-en-1-yl)oxy)dimethylsilane

: 100-52-7
benzaldehyde

: 14366-89-3,17226-79-8,36041-80-2,76549-03-6,76549-05-8,94199-26-5,99210-93-2,99210-95-4,34880-62-1
methyl 3-hydroxy-2-methyl-3-phenylpropanoate

Guidance literature:: With scandium tris(trifluoromethanesulfonate); 1-dodecyloxy-4-(heptadecafluorooctyl)benzene; In carbon dioxide; at 50 ℃; for 3h; under 60006 Torr;
DOI:10.1021/ol0173127

Reference yield: 95.0%

: 100-52-7
benzaldehyde

: 292638-85-8,9003-21-8,96-33-3
acrylic acid methyl ester

: 14366-89-3,17226-79-8,36041-80-2,76549-03-6,76549-05-8,94199-26-5,99210-93-2,99210-95-4,34880-62-1
methyl 3-hydroxy-2-methyl-3-phenylpropanoate

Guidance literature:: With Wilkinson's catalyst; diethylzinc; In tetrahydrofuran; hexane; at 0 ℃; for 3h; Inert atmosphere;
DOI:10.1002/adsc.201100463

Reference yield: 94.0%

: 100-52-7
benzaldehyde

: 292638-85-8,9003-21-8,96-33-3
acrylic acid methyl ester

: 14366-89-3,76549-03-6,17226-79-8,34880-62-1,36041-80-2,76549-05-8,94199-26-5,99210-93-2,99210-95-4
methyl 3-hydroxy-2-methyl-3-phenylpropanoate

Guidance literature:: acrylic acid methyl ester; With chloro(1,5-cyclooctadiene)rhodium(I) dimer; 1,2-bis(2,5-dimethylphospholano)benzene; dichloromethylsilane; In diethyl ether; at 20 ℃; for 1.5h;

benzaldehyde; In diethyl ether; at -46 ℃; for 4h; Further stages.;
DOI:10.1021/ol016279l