[1,2-bis(diphenylphosphino-k.P,P')ethane](N,N'-iminodiethylenebis(phthalimide)dithiocarbamato)nickel(II) tetraphenylborate monohydrate

Base Information

Chemical Name:[1,2-bis(diphenylphosphino-k.P,P')ethane](N,N'-iminodiethylenebis(phthalimide)dithiocarbamato)nickel(II) tetraphenylborate monohydrate
CAS No.:190122-16-8
Molecular Formula:C₂₄H₂₀B*C₄₇H₄₀N₃NiO₄P₂S₂*H₂O
Molecular Weight:1232.87
Hs Code.:

[1,2-bis(diphenylphosphino-k.P,P')ethane](N,N'-iminodiethylenebis(phthalimide)dithiocarbamato)nickel(II) tetraphenylborate monohydrate

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Chemical Property of [1,2-bis(diphenylphosphino-k.P,P')ethane](N,N'-iminodiethylenebis(phthalimide)dithiocarbamato)nickel(II) tetraphenylborate monohydrate

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Technology Process of [1,2-bis(diphenylphosphino-k.P,P')ethane](N,N'-iminodiethylenebis(phthalimide)dithiocarbamato)nickel(II) tetraphenylborate monohydrate

There total 2 articles about [1,2-bis(diphenylphosphino-k.P,P')ethane](N,N'-iminodiethylenebis(phthalimide)dithiocarbamato)nickel(II) tetraphenylborate monohydrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: bis(N,N'-iminodiethylenebis(phthalimide)dithiocarbamato)nickel(II)

: 143-66-8
sodium tetraphenyl borate

: 1663-45-2
1,2-bis-(diphenylphosphino)ethane

: 190122-16-8
[1,2-bis(diphenylphosphino-k.P,P')ethane](N,N'-iminodiethylenebis(phthalimide)dithiocarbamato)nickel(II) tetraphenylborate monohydrate

Guidance literature:: In acetonitrile; equimolar amts., refluxing for 3 h; filtration, concn., standing for 3 d, collection (filtration), drying (over CaCl2), recrystn. (MeCN);
DOI:10.1016/s0020-1693(96)05447-3

Reference yield:

: 63563-83-7
bis(phthalimidylethyl)amine

: 190122-16-8
[1,2-bis(diphenylphosphino-k.P,P')ethane](N,N'-iminodiethylenebis(phthalimide)dithiocarbamato)nickel(II) tetraphenylborate monohydrate

Guidance literature:: Multi-step reaction with 2 steps

1: water; acetonitrile

2: acetonitrile

In water; acetonitrile;
DOI:10.1016/s0020-1693(96)05447-3