(1S,2S,4aS,5S,6S,8S,8aR)-5-Methoxymethoxy-1,6,8-trimethyl-2-((E)-1-methyl-3-phenylsulfanyl-propenyl)-1,2,4a,5,6,7,8,8a-octahydro-naphthalene-1-carbaldehyde

Base Information

• Chemical Name: (1S,2S,4aS,5S,6S,8S,8aR)-5-Methoxymethoxy-1,6,8-trimethyl-2-((E)-1-methyl-3-phenylsulfanyl-propenyl)-1,2,4a,5,6,7,8,8a-octahydro-naphthalene-1-carbaldehyde
• CAS No.: 138213-59-9
• Molecular Formula: C₂₆H₃₆O₃S
• Molecular Weight: 428.636

Synonyms:

Chemical Property of (1S,2S,4aS,5S,6S,8S,8aR)-5-Methoxymethoxy-1,6,8-trimethyl-2-((E)-1-methyl-3-phenylsulfanyl-propenyl)-1,2,4a,5,6,7,8,8a-octahydro-naphthalene-1-carbaldehyde

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (1S,2S,4aS,5S,6S,8S,8aR)-5-Methoxymethoxy-1,6,8-trimethyl-2-((E)-1-methyl-3-phenylsulfanyl-propenyl)-1,2,4a,5,6,7,8,8a-octahydro-naphthalene-1-carbaldehyde

There total 3 articles about (1S,2S,4aS,5S,6S,8S,8aR)-5-Methoxymethoxy-1,6,8-trimethyl-2-((E)-1-methyl-3-phenylsulfanyl-propenyl)-1,2,4a,5,6,7,8,8a-octahydro-naphthalene-1-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(E)-(2S,3S,5S)-8-(1-Ethoxy-ethoxy)-2-methoxymethoxy-3,5,7-trimethyl-oct-6-en-1-ol (138194-37-3) → (1S,2S,4aS,5S,6S,8S,8aR)-5-Methoxymethoxy-1,6,8-trimethyl-2-((E)-1-methyl-3-phenylsulfanyl-propenyl)-1,2,4a,5,6,7,8,8a-octahydro-naphthalene-1-carbaldehyde (138213-59-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 92 percent / N-methylmorpholine-N-oxide, MS 4A, / n-Pr₄NRuO₄ / CH₂Cl₂ / Ambient temperature

With 4-methylmorpholine N-oxide; tetrapropylammonium perruthennate; In dichloromethane;

DOI:10.1016/S0040-4039(00)93498-1

Reference yield:

tert-Butyl-[(E)-(2S,3S,5S)-8-(1-ethoxy-ethoxy)-2-methoxymethoxy-3,5,7-trimethyl-oct-6-enyloxy]-dimethyl-silane → (1S,2S,4aS,5S,6S,8S,8aR)-5-Methoxymethoxy-1,6,8-trimethyl-2-((E)-1-methyl-3-phenylsulfanyl-propenyl)-1,2,4a,5,6,7,8,8a-octahydro-naphthalene-1-carbaldehyde (138213-59-9)

Guidance literature:

Multi-step reaction with 3 steps

1: nBu₄NF / tetrahydrofuran / Ambient temperature

2: 92 percent / N-methylmorpholine-N-oxide, MS 4A, / n-Pr₄NRuO₄ / CH₂Cl₂ / Ambient temperature

With tetrabutyl ammonium fluoride; 4-methylmorpholine N-oxide; tetrapropylammonium perruthennate; In tetrahydrofuran; dichloromethane;

DOI:10.1016/S0040-4039(00)93498-1

Reference yield:

(E)-(2S,3S,5S)-8-(1-Ethoxy-ethoxy)-2-methoxymethoxy-3,5,7-trimethyl-oct-6-enal + diphenyldisulfane (882-33-7) → (1S,2S,4aS,5S,6S,8S,8aR)-5-Methoxymethoxy-1,6,8-trimethyl-2-((E)-1-methyl-3-phenylsulfanyl-propenyl)-1,2,4a,5,6,7,8,8a-octahydro-naphthalene-1-carbaldehyde (138213-59-9)

Guidance literature:

Multistep reaction;

DOI:10.1016/S0040-4039(00)93498-1

upstream raw materials:

diphenyldisulfane

(E)-(2S,3S,5S)-8-(1-Ethoxy-ethoxy)-2-methoxymethoxy-3,5,7-trimethyl-oct-6-en-1-ol

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