TETRAKIS(3-AMINOPROPYL)-1,3-PROPANEDIAMINE

Base Information

• Chemical Name: TETRAKIS(3-AMINOPROPYL)-1,3-PROPANEDIAMINE
• CAS No.: 121263-90-9
• Molecular Formula: C15H38N6
• Molecular Weight: 302.50200
• Mol file: 121263-90-9.mol

Synonyms:tetrakis(3-aminopropyl)-1,3-propanediamine;N,N,N',N'-tetrakis(3-aminopropyl)-1,3-propylenediamine;N,N,N',N'-tetrakis(3-aminopropyl)-1,3-propanediamine;N,N,N',N'-tetrakis(aminopropyl)trimethylenediamine;N-(3-aminopropyl)-N-{3-[bis(3-aminopropyl)amino]propyl}-1,3-propanediamine;1,3-Propanediamine,N,N,N',N'-tetrakis(3-aminopropyl);

Chemical Property of TETRAKIS(3-AMINOPROPYL)-1,3-PROPANEDIAMINE

Chemical Property:

• PSA: 110.56000
• LogP: 2.17690

Purity/Quality:

99% ^*data from raw suppliers

TETRAKIS-(3-AMINOPROPYL)-1,3-PROPANEDIAMINE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of TETRAKIS(3-AMINOPROPYL)-1,3-PROPANEDIAMINE

There total 4 articles about TETRAKIS(3-AMINOPROPYL)-1,3-PROPANEDIAMINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

3,3',3'',3'''-[1,3-propanediyldi(nitrilo)]tetrapropanenitrile → N1,N1,N3,N3-tetrakis(3-aminopropyl)propane-1,3-diamine (121263-90-9)

Guidance literature:

With hydrogen; sodium hydroxide; In tetrahydrofuran; ethanol; water; at 20 ℃; for 24h; under 760.051 Torr;

Reference yield: 70.0%

N1,N1,N3,N3-tetrakis(3-azidopropyl)propane-1,3-diamine → N1,N1,N3,N3-tetrakis(3-aminopropyl)propane-1,3-diamine (121263-90-9)

Guidance literature:

With triphenylphosphine; In tetrahydrofuran; water; at 70 ℃; for 48h;

DOI:10.1021/jacs.7b00235

Reference yield:

bis-(3-hydroxypropyl)amine (14002-33-6) → N1,N1,N3,N3-tetrakis(3-aminopropyl)propane-1,3-diamine (121263-90-9)

Guidance literature:

Multi-step reaction with 4 steps

1: thionyl chloride / chloroform / 24 h / 0 - 20 °C

2: sodium azide / water / 24 h / 80 °C

3: potassium carbonate / acetonitrile / 48 h / 80 °C

4: triphenylphosphine / tetrahydrofuran; water / 48 h / 70 °C

With thionyl chloride; sodium azide; potassium carbonate; triphenylphosphine; In tetrahydrofuran; chloroform; water; acetonitrile;

DOI:10.1021/jacs.7b00235

upstream raw materials:

bis-(3-hydroxypropyl)amine

di-(3-chloropropyl)amine

Downstream raw materials:

C₈₇H₁₀₂N₆O₁₂