β-(4-Cyanphenyl)ethylacetaminomalonsaeurediethylester

Base Information

Chemical Name:β-(4-Cyanphenyl)ethylacetaminomalonsaeurediethylester
CAS No.:82098-50-8
Molecular Formula:C₁₈H₂₂N₂O₅
Molecular Weight:346.383
Hs Code.:

Synonyms:

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Chemical Property of β-(4-Cyanphenyl)ethylacetaminomalonsaeurediethylester

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Technology Process of β-(4-Cyanphenyl)ethylacetaminomalonsaeurediethylester

There total 4 articles about β-(4-Cyanphenyl)ethylacetaminomalonsaeurediethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-27-6
2-(4-nitrophenyl)ethanol

: 82098-50-8
β-(4-Cyanphenyl)ethylacetaminomalonsaeurediethylester

Guidance literature:: Multi-step reaction with 4 steps

1: 70 percent / H₂ / Raney-nickel / methanol / Ambient temperature

2: 1.) NaNO₂/conc. HCl; 2.) CuCN/NaCN / 1.) H₂O, 0-5 deg C; 2.) benzene, 0-5 deg C, 30 min; room temp., 4 h

3: 63 percent / PBr₃ / CHCl₃ / 1.5 h / Heating

4: 1.) KI; 2.) Na / 1.) EtOH, reflux; 2.) EtOH, reflux, 5 h

With hydrogenchloride; sodium cyanide; hydrogen; sodium; phosphorus tribromide; potassium iodide; sodium nitrite; nickel; In methanol; chloroform;

Reference yield:

: 69395-13-7
4-(2-hydroxyethyl)benzonitrile

: 82098-50-8
β-(4-Cyanphenyl)ethylacetaminomalonsaeurediethylester

Guidance literature:: Multi-step reaction with 2 steps

1: 63 percent / PBr₃ / CHCl₃ / 1.5 h / Heating

2: 1.) KI; 2.) Na / 1.) EtOH, reflux; 2.) EtOH, reflux, 5 h

With sodium; phosphorus tribromide; potassium iodide; In chloroform;

Reference yield:

: 104-10-9
2-(4'-aminophenyl)ethyl alcohol

: 82098-50-8
β-(4-Cyanphenyl)ethylacetaminomalonsaeurediethylester

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) NaNO₂/conc. HCl; 2.) CuCN/NaCN / 1.) H₂O, 0-5 deg C; 2.) benzene, 0-5 deg C, 30 min; room temp., 4 h

2: 63 percent / PBr₃ / CHCl₃ / 1.5 h / Heating

3: 1.) KI; 2.) Na / 1.) EtOH, reflux; 2.) EtOH, reflux, 5 h

With hydrogenchloride; sodium cyanide; sodium; phosphorus tribromide; potassium iodide; sodium nitrite; In chloroform;