2H-1-benzyloxycarbonyl-2-phenyl-4-methyl-pyridine

Base Information

Chemical Name:2H-1-benzyloxycarbonyl-2-phenyl-4-methyl-pyridine
CAS No.:104704-53-2
Molecular Formula:C₂₀H₁₉NO₂
Molecular Weight:305.376
Hs Code.:

Synonyms:

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Chemical Property of 2H-1-benzyloxycarbonyl-2-phenyl-4-methyl-pyridine

Chemical Property:

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Technology Process of 2H-1-benzyloxycarbonyl-2-phenyl-4-methyl-pyridine

There total 1 articles about 2H-1-benzyloxycarbonyl-2-phenyl-4-methyl-pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108-89-4
picoline

: phenylmagnesium bromide

: 501-53-1,94274-21-2
benzyl chloroformate

: 104704-53-2
2H-1-benzyloxycarbonyl-2-phenyl-4-methyl-pyridine

Guidance literature:: Multistep reaction; 1.) -5 degC, THF, toluene, 2 h; 2.) room temp., 1 h;
DOI:10.1248/cpb.33.4572

Reference yield:

: 104704-53-2
2H-1-benzyloxycarbonyl-2-phenyl-4-methyl-pyridine

: 104704-74-7
4-benzyloxycarbonyl-4,5-dihydro-5-phenyl-7-methyl-1,4-oxazepine

Guidance literature:: Multi-step reaction with 3 steps

1: CH₂Cl₂ / Irradiation

2: 80 percent / m-chloroperbenzoic acid / CH₂Cl₂ / Ambient temperature

3: 72 percent / toluene / Heating

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; toluene;
DOI:10.1248/cpb.33.4572

Reference yield:

: 104704-53-2
2H-1-benzyloxycarbonyl-2-phenyl-4-methyl-pyridine

: 104704-80-5
1-ethyloxycarbonyl-4-benzyloxycarbonyl-4,5-dihydro-5-ethyl-7-methyl-1,4-diazepine

Guidance literature:: Multi-step reaction with 3 steps

1: CH₂Cl₂ / Irradiation

2: 28 percent / triethylbenzylammonium bromide, sodium hydrogencarbonate / CH₂Cl₂ / 5 h

3: 57 percent / xylene / Heating

With benzyltriethylammonium bromide; sodium hydrogencarbonate; In dichloromethane; xylene;
DOI:10.1248/cpb.33.4572