chloro-hydrido-9-methylguanine-bis-(triphenylphosphine)-iridium(III)-tetrafluoroborate

Base Information

Chemical Name:chloro-hydrido-9-methylguanine-bis-(triphenylphosphine)-iridium(III)-tetrafluoroborate
CAS No.:99626-35-4
Molecular Formula:BF₄*C₄₂H₃₈ClIrN₅OP₂
Molecular Weight:1005.22
Hs Code.:

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Chemical Property of chloro-hydrido-9-methylguanine-bis-(triphenylphosphine)-iridium(III)-tetrafluoroborate

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Technology Process of chloro-hydrido-9-methylguanine-bis-(triphenylphosphine)-iridium(III)-tetrafluoroborate

There total 1 articles about chloro-hydrido-9-methylguanine-bis-(triphenylphosphine)-iridium(III)-tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 79470-05-6
((C₆H₅)3P)2(Cl)(N₂)(H)IrFBF₃

: 5502-78-3,137609-04-2
9-Methylguanine

: 99626-35-4
chloro-hydrido-9-methylguanine-bis-(triphenylphosphine)-iridium(III)-tetrafluoroborate

Guidance literature:: In dichloromethane; byproducts: N2; (Ar); mixt. dried (-10°C; high vac.); added at -20°C cooled CH2Cl2; stirred (-25°C; 48 h); stirred (room temp.; 1 h); ppt.; centred; washed (CH2Cl2; two time n-pentane); dried (high vac.; 3 h); dissolved in methanol; filtered; pptd. with Et2O and n-pentane; centrifuged; washed with pentane; dried in high vac.; elem. anal.;