C₈H₁₄BOCOCH((C₆H₅))NH₂

Base Information

Chemical Name:C₈H₁₄BOCOCH((C₆H₅))NH₂
CAS No.:117256-66-3
Molecular Formula:C₁₆H₂₂BNO₂
Molecular Weight:271.167
Hs Code.:

C<sub>8</sub>H<sub>14</sub>BOCOCH((C<sub>6</sub>H<sub>5</sub>))NH<sub>2</sub>

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₈H₁₄BOCOCH((C₆H₅))NH₂

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Technology Process of C₈H₁₄BOCOCH((C₆H₅))NH₂

There total 1 articles about C₈H₁₄BOCOCH((C₆H₅))NH₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 38050-71-4
9-methoxy-9-BBN

: 2835-06-5
phenylglycin

: 117256-66-3
C₈H₁₄BOCOCH((C₆H₅))NH₂

Guidance literature:: In tetrahydrofuran; ethanol; water; dropwise addn. of 1 M soln. of C8H14BOCH3 in THF to phenylglycine in ethanol/H2O (1:1), stirring at 80-100°C; control of completion of the reaction by (11)B-NMR, removing of solvent under vacuum (1-2.0 mm), treating with methanol, filtration, washing with hexane or ether;
DOI:10.1016/0022-328X(88)89064-8