β-(cyclohexenyl-1)-vinyl ethyl ether

Base Information

Chemical Name:β-(cyclohexenyl-1)-vinyl ethyl ether
CAS No.:39556-59-7
Molecular Formula:C₁₀H₁₆O
Molecular Weight:152.236
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of β-(cyclohexenyl-1)-vinyl ethyl ether

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Technology Process of β-(cyclohexenyl-1)-vinyl ethyl ether

There total 2 articles about β-(cyclohexenyl-1)-vinyl ethyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 77570-38-8
1-ethoxy-1-(2'2'-diethoxyethyl)cyclohexane

: 39556-59-7
β-(cyclohexenyl-1)-vinyl ethyl ether

Guidance literature:: With ammonium dihydrogen phosphate; at 260 - 280 ℃; for 1h;
DOI:10.1007/BF00696716

Reference yield:

: 1670-47-9
1,1-diethoxycyclohexane

: 39556-59-7
β-(cyclohexenyl-1)-vinyl ethyl ether

Guidance literature:: Multi-step reaction with 2 steps

1: 62 percent / BF₃*OEt₂ / 1.) 0 deg C, 1 h, 2.) 20 deg C, 1,5 h

2: 51 percent / NH₄H₂PO₄ / 1 h / 260 - 280 °C

With ammonium dihydrogen phosphate; boron trifluoride diethyl etherate;
DOI:10.1007/BF00696716