(6R)-8-oxo-7t-(2-thiophen-2-yl-acetylamino)-(6rH)-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2,3-dicarboxylic acid 2-benzhydryl ester 3-methyl ester

Base Information

Chemical Name:(6R)-8-oxo-7t-(2-thiophen-2-yl-acetylamino)-(6rH)-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2,3-dicarboxylic acid 2-benzhydryl ester 3-methyl ester
CAS No.:55243-83-9
Molecular Formula:C₂₈H₂₄N₂O₆S₂
Molecular Weight:548.64
Hs Code.:

(6<i>R</i>)-8-oxo-7<i>t</i>-(2-thiophen-2-yl-acetylamino)-(6<i>r</i><i>H</i>)-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2,3-dicarboxylic acid 2-benzhydryl ester 3-methyl ester

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Chemical Property of (6R)-8-oxo-7t-(2-thiophen-2-yl-acetylamino)-(6rH)-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2,3-dicarboxylic acid 2-benzhydryl ester 3-methyl ester

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Technology Process of (6R)-8-oxo-7t-(2-thiophen-2-yl-acetylamino)-(6rH)-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2,3-dicarboxylic acid 2-benzhydryl ester 3-methyl ester

There total 5 articles about (6R)-8-oxo-7t-(2-thiophen-2-yl-acetylamino)-(6rH)-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2,3-dicarboxylic acid 2-benzhydryl ester 3-methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 55331-32-3
(6R)-3-formyl-8-oxo-7t-(2-thiophen-2-yl-acetylamino)-(6rH)-5-thia-1-aza-bicyclo[4.2.0]oct-3-ene-2c-carboxylic acid benzhydryl ester

: 55243-83-9
(6R)-8-oxo-7t-(2-thiophen-2-yl-acetylamino)-(6rH)-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2,3-dicarboxylic acid 2-benzhydryl ester 3-methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: TsOH / benzene

2: NBS, AIBN / benzene

3: (i) NaI, acetone, (ii) Zn, AcOH

4: (i) , (ii) (oxidation), (iii) (reduction)

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); toluene-4-sulfonic acid; In benzene;
DOI:10.1039/c39740001012

Reference yield:

: 55243-79-3
(6R)-3-[1,3]dioxolan-2-yl-8-oxo-7t-(2-thiophen-2-yl-acetylamino)-(6rH)-5-thia-1-aza-bicyclo[4.2.0]oct-3-ene-2c-carboxylic acid benzhydryl ester

: 55243-83-9
(6R)-8-oxo-7t-(2-thiophen-2-yl-acetylamino)-(6rH)-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2,3-dicarboxylic acid 2-benzhydryl ester 3-methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: NBS, AIBN / benzene

2: (i) NaI, acetone, (ii) Zn, AcOH

3: (i) , (ii) (oxidation), (iii) (reduction)

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); In benzene;
DOI:10.1039/c39740001012

Reference yield:

: 55243-80-6
(6R)-8-oxo-7t-(2-thiophen-2-yl-acetylamino)-(6rH)-5-thia-1-aza-bicyclo[4.2.0]oct-3-ene-2c,3-dicarboxylic acid 2-benzhydryl ester 3-(2-bromo-ethyl) ester

: 55243-83-9
(6R)-8-oxo-7t-(2-thiophen-2-yl-acetylamino)-(6rH)-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2,3-dicarboxylic acid 2-benzhydryl ester 3-methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: (i) NaI, acetone, (ii) Zn, AcOH

2: (i) , (ii) (oxidation), (iii) (reduction)

DOI:10.1039/c39740001012