Technology Process of C45H78N2O12
There total 4 articles about C45H78N2O12 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium cyanoborohydride; acetic acid;
In
N,N-dimethyl-formamide;
Inert atmosphere;
DOI:10.1021/jm101593u
- Guidance literature:
-
Multi-step reaction with 4 steps
1: hydroxylamine; acetic acid / water; isopropyl alcohol / 120 h / 40 °C / Inert atmosphere
2: pyridine / tetrahydrofuran / 20 h / 40 °C / Inert atmosphere
3: sodium tetrahydroborate; acetic acid / methanol / Inert atmosphere
4: sodium cyanoborohydride; acetic acid / N,N-dimethyl-formamide / Inert atmosphere
With
pyridine; sodium tetrahydroborate; hydroxylamine; sodium cyanoborohydride; acetic acid;
In
tetrahydrofuran; methanol; water; N,N-dimethyl-formamide; isopropyl alcohol;
3: Beckmann rearrangement;
DOI:10.1021/jm101593u
- Guidance literature:
-
Multi-step reaction with 3 steps
1: pyridine / tetrahydrofuran / 20 h / 40 °C / Inert atmosphere
2: sodium tetrahydroborate; acetic acid / methanol / Inert atmosphere
3: sodium cyanoborohydride; acetic acid / N,N-dimethyl-formamide / Inert atmosphere
With
pyridine; sodium tetrahydroborate; sodium cyanoborohydride; acetic acid;
In
tetrahydrofuran; methanol; N,N-dimethyl-formamide;
2: Beckmann rearrangement;
DOI:10.1021/jm101593u
