Technology Process of C24H26N2O2
There total 4 articles about C24H26N2O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
trifluoroacetic acid;
In
dichloromethane;
at 20 ℃;
for 0.5h;
Inert atmosphere;
DOI:10.1021/jm2001053
- Guidance literature:
-
Multi-step reaction with 2 steps
1: ammonium acetate / 5,5-dimethyl-1,3-cyclohexadiene / 7 h / Reflux; Molecular sieve; Inert atmosphere
2: trifluoroacetic acid / dichloromethane / 0.5 h / 20 °C / Inert atmosphere
With
ammonium acetate; trifluoroacetic acid;
In
5,5-dimethyl-1,3-cyclohexadiene; dichloromethane;
DOI:10.1021/jm2001053
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: dmap / tetrahydrofuran; tert-butyl alcohol / 24 h / Reflux; Inert atmosphere
2.1: caesium carbonate / ethanol / 0.1 h / 20 °C / Sonication; Inert atmosphere
2.2: 12 h / 20 °C / Inert atmosphere
3.1: ammonium acetate / 5,5-dimethyl-1,3-cyclohexadiene / 7 h / Reflux; Molecular sieve; Inert atmosphere
4.1: trifluoroacetic acid / dichloromethane / 0.5 h / 20 °C / Inert atmosphere
With
dmap; ammonium acetate; caesium carbonate; trifluoroacetic acid;
In
tetrahydrofuran; 5,5-dimethyl-1,3-cyclohexadiene; ethanol; dichloromethane; tert-butyl alcohol;
DOI:10.1021/jm2001053
