C₃₈H₅₄N₈O₈S₂

Base Information

• Chemical Name: C₃₈H₅₄N₈O₈S₂
• CAS No.: 219931-72-3
• Molecular Formula: C₃₈H₅₄N₈O₈S₂
• Molecular Weight: 815.028
• Mol file: 219931-72-3.mol

Synonyms:

Chemical Property of C₃₈H₅₄N₈O₈S₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₈H₅₄N₈O₈S₂

There total 8 articles about C₃₈H₅₄N₈O₈S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-[3-(dimethylamino)propyl]-1-methyl-4-{[(1-methyl-4-nitro-1H-pyrrol-2-yl)carbonyl]amino}-1H-pyrrole-2-carboxamide (65361-31-1) → C38H54N8O8S2 (219931-72-3)

Guidance literature:

Multi-step reaction with 2 steps

1: H₂ / Pd/C / methanol / 2 h

2: HOBR, EDCI / dimethylformamide / 14 h / Ambient temperature

With hydrogen; hypobromous acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide;

DOI:10.1021/jo9812072

Reference yield:

(2S)-2-[di(ethylsulfanyl)methyl]tetrahydro-1H-pyrrole (105089-88-1) → C38H54N8O8S2 (219931-72-3)

Guidance literature:

Multi-step reaction with 3 steps

1: Et₃N / CH₂Cl₂ / 1 h / 0 °C

2: NaOH / ethanol / 18 h / 50 °C

3: HOBR, EDCI / dimethylformamide / 14 h / Ambient temperature

With sodium hydroxide; hypobromous acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In ethanol; dichloromethane; N,N-dimethyl-formamide;

DOI:10.1021/jo9812072

Reference yield:

vanillin (121-33-5,8014-42-4) → C38H54N8O8S2 (219931-72-3)

Guidance literature:

Multi-step reaction with 7 steps

1: K₂CO₃ / tetrahydrofuran

2: HNO₃, SnCl₄ / CH₂Cl₂

3: sodium chlorite, sulfamic acid / H₂O

4: SOCl₂ / benzene / 2 h / Ambient temperature

5: Et₃N / CH₂Cl₂ / 1 h / 0 °C

6: NaOH / ethanol / 18 h / 50 °C

7: HOBR, EDCI / dimethylformamide / 14 h / Ambient temperature

With sodium hydroxide; sodium chlorite; thionyl chloride; aminosulfonic acid; nitric acid; hypobromous acid; tin(IV) chloride; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; ethanol; dichloromethane; water; N,N-dimethyl-formamide; benzene;

DOI:10.1021/jo9812072

upstream raw materials:

(2S)-2-[di(ethylsulfanyl)methyl]tetrahydro-1H-pyrrole

N-[3-(dimethylamino)propyl]-1-methyl-4-{[(1-methyl-4-nitro-1H-pyrrol-2-yl)carbonyl]amino}-1H-pyrrole-2-carboxamide

vanillin

ethyl 4-(4-formyl-2-methoxyphenoxy)butanoate