Salicylaldehyde monobutyl hydrazone

Base Information

• Chemical Name: Salicylaldehyde monobutyl hydrazone
• CAS No.: 84646-19-5
• Molecular Formula: C₁₁H₁₆N₂O
• Molecular Weight: 192.261
• Mol file: 84646-19-5.mol

Synonyms:

Chemical Property of Salicylaldehyde monobutyl hydrazone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Salicylaldehyde monobutyl hydrazone

There total 2 articles about Salicylaldehyde monobutyl hydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

butylhydrazine (3530-11-8) + salicylaldehyde (90-02-8) → Salicylaldehyde monobutyl hydrazone (84646-19-5)

Guidance literature:

In benzene; 1) mixing below 15 deg C, 2) room temp., 1 h.;

DOI:10.1007/BF00503181

Reference yield:

→ Salicylaldehyde monobutyl hydrazone (84646-19-5)

Guidance literature:

Salicylaldehyd, Butylhydrazin, Benzol;

Reference yield: 48.0%

Salicylaldehyde monobutyl hydrazone (84646-19-5) + benzaldehyde (100-52-7) → 3-Butyl-2-phenyl-6,7-benzo-2,3-dihydro-1,3,4-oxadiazepine (84646-21-9)

Guidance literature:

at 70 ℃; for 2h;

DOI:10.1007/BF00503181

upstream raw materials:

butylhydrazine

salicylaldehyde

Downstream raw materials:

3-Butyl-2-phenyl-6,7-benzo-2,3-dihydro-1,3,4-oxadiazepine

3-Butyl-2-(2-hydroxyphenyl)-6,7-benzo-2,3-dihydro-1,3,4-oxadiazepine