[Ru(η5-C5H5)(1,2-bis(diphenylphosphino)ethane)(2-azidophenyl isocyanide)]Cl

Base Information

Chemical Name:[Ru(η5-C5H5)(1,2-bis(diphenylphosphino)ethane)(2-azidophenyl isocyanide)]Cl
CAS No.:1201128-96-2
Molecular Formula:C₃₈H₃₃N₄P₂Ru*Cl
Molecular Weight:744.177
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [Ru(η5-C5H5)(1,2-bis(diphenylphosphino)ethane)(2-azidophenyl isocyanide)]Cl

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Technology Process of [Ru(η5-C5H5)(1,2-bis(diphenylphosphino)ethane)(2-azidophenyl isocyanide)]Cl

There total 1 articles about [Ru(η5-C5H5)(1,2-bis(diphenylphosphino)ethane)(2-azidophenyl isocyanide)]Cl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: chlorocyclopentadienylbis(triphenylphosphine)ruthenium(II)

: 86652-69-9
2-azido-4-(tert-butyl)-1-isocyanobenzene

: 1201128-96-2
[Ru(η5-C5H5)(1,2-bis(diphenylphosphino)ethane)(2-azidophenyl isocyanide)]Cl

Guidance literature:: In methanol; (Ar); Schlenk technique; ligand (1.05 equiv.) was added to suspn. of Ru complex (1 equiv.) in MeOH; stirred under reflux for 12 h; evapd. (vac.); washed (Et2O); elem. anal.;
DOI:10.1039/b915033a

Reference yield: 93.0%

: 1201128-96-2
[Ru(η5-C5H5)(1,2-bis(diphenylphosphino)ethane)(2-azidophenyl isocyanide)]Cl

: ammonium chloride

: 143-66-8
sodium tetraphenyl borate

: [Ru(η5-C5H5)(1,2-bis(diphenylphosphino)ethane)(benzimidazolin-2-ylidene)]BPh4

Guidance literature:: With Zn; In methanol; water; (Ar); Schlenk technique; mixt. of Ru complex (1 equiv.), Zn (1.3 equiv.)and NH4Cl (2.3 equiv.) in MeOH/H2O was stirred under reflux for 24 h; evapd. (vac.); CH2Cl2 added; filtered; solvent removed (vac.); NaBPh4 added; elem. anal.;
DOI:10.1039/b915033a