Technology Process of Benzo[b]thiophene-2-carboxylic acid, 5-methoxy-3-phenoxy-, phenyl
ester
There total 5 articles about Benzo[b]thiophene-2-carboxylic acid, 5-methoxy-3-phenoxy-, phenyl
ester which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
Tris(3,6-dioxaheptyl)amine; sodium hydride;
Yield given. Multistep reaction;
DOI:10.1021/jm00083a023
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: pyridine; dmap / dichloromethane / 6 h / 20 °C
2.1: dihydrogen peroxide; trifluoroacetic acid / dichloromethane; water / 1.75 h / 0 - 20 °C
3.1: sodium hydride / 1,4-dioxane / 0.25 h / 20 °C
3.2: 0.5 h / 20 °C
4.1: chloro-trimethyl-silane; sodium iodide / acetonitrile / 0.25 h / 0 - 20 °C
With
pyridine; dmap; chloro-trimethyl-silane; dihydrogen peroxide; sodium hydride; trifluoroacetic acid; sodium iodide;
In
1,4-dioxane; dichloromethane; water; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: dihydrogen peroxide; trifluoroacetic acid / dichloromethane; water / 1.75 h / 0 - 20 °C
2.1: sodium hydride / 1,4-dioxane / 0.25 h / 20 °C
2.2: 0.5 h / 20 °C
3.1: chloro-trimethyl-silane; sodium iodide / acetonitrile / 0.25 h / 0 - 20 °C
With
chloro-trimethyl-silane; dihydrogen peroxide; sodium hydride; trifluoroacetic acid; sodium iodide;
In
1,4-dioxane; dichloromethane; water; acetonitrile;
![3-chloro-5-methoxybenzo[b]thiophene-2-carbonyl chloride](/Databaselist/images/loading.webp)
