SnPh₂Cl(1,2-bis(1H-benzimidazol-2-yl)ethane-1,2-diol(-1H))

Base Information

• Chemical Name: SnPh₂Cl(1,2-bis(1H-benzimidazol-2-yl)ethane-1,2-diol(-1H))
• CAS No.: 1345456-47-4
• Molecular Formula: C₂₈H₂₃ClN₄O₂Sn
• Molecular Weight: 601.679
• Mol file: 1345456-47-4.mol

Synonyms:

Chemical Property of SnPh₂Cl(1,2-bis(1H-benzimidazol-2-yl)ethane-1,2-diol(-1H))

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of SnPh₂Cl(1,2-bis(1H-benzimidazol-2-yl)ethane-1,2-diol(-1H))

There total 1 articles about SnPh₂Cl(1,2-bis(1H-benzimidazol-2-yl)ethane-1,2-diol(-1H)) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

1,2-bis(1H-benzo[d]imidazol-2-yl)ethane-1,2-diol (3314-32-7) + diphenyltin(IV) dichloride (1135-99-5) → SnPh2Cl(1,2-bis(1H-benzimidazol-2-yl)ethane-1,2-diol(-1H)) (1345456-47-4)

Guidance literature:

In methanol; to stirred soln. of Ph2SnCl2 in MeOH added 1,2-bis(1H-benzimidazol-2-yl)ethane-1,2-diol; react. mixt. refluxed at 80°C with stirring on rota mantle for 4 h; allowed to stand at room temp. overnight; slowly evapd.; washed with hexane; dried in vacuo; elem. anal.;

DOI:10.1016/j.jorganchem.2011.08.007

upstream raw materials:

1,2-bis(1H-benzo[d]imidazol-2-yl)ethane-1,2-diol

diphenyltin(IV) dichloride