[chloro-η4-(1,5-cyclooctadiene)-κ-P-(1-(diphenyl(2-diphenylphosphinoethyl)phosphonio)-3-triphenylphosphoniobenzo[c]phospholide)rhodium(I)]Tetraphenylborate

Base Information

Chemical Name:[chloro-η4-(1,5-cyclooctadiene)-κ-P-(1-(diphenyl(2-diphenylphosphinoethyl)phosphonio)-3-triphenylphosphoniobenzo[c]phospholide)rhodium(I)]Tetraphenylborate
CAS No.:351203-69-5
Molecular Formula:C₂₄H₂₀B*C₆₀H₅₅ClP₄Rh
Molecular Weight:1357.58
Hs Code.:

[chloro-η4-(1,5-cyclooctadiene)-κ-P-(1-(diphenyl(2-diphenylphosphinoethyl)phosphonio)-3-triphenylphosphoniobenzo[c]phospholide)rhodium(I)]Tetraphenylborate

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Chemical Property of [chloro-η4-(1,5-cyclooctadiene)-κ-P-(1-(diphenyl(2-diphenylphosphinoethyl)phosphonio)-3-triphenylphosphoniobenzo[c]phospholide)rhodium(I)]Tetraphenylborate

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Technology Process of [chloro-η4-(1,5-cyclooctadiene)-κ-P-(1-(diphenyl(2-diphenylphosphinoethyl)phosphonio)-3-triphenylphosphoniobenzo[c]phospholide)rhodium(I)]Tetraphenylborate

There total 2 articles about [chloro-η4-(1,5-cyclooctadiene)-κ-P-(1-(diphenyl(2-diphenylphosphinoethyl)phosphonio)-3-triphenylphosphoniobenzo[c]phospholide)rhodium(I)]Tetraphenylborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: bis[μ-chloro-κ2-P,P'-(1-(diphenyl(2-diphenylphosphinoethyl)phosphonio)-3-triphenylphosphoniobenzo[c]phospholide)rhodium(I)]Bistetraphenylborate*tetrahydrofuran

: 5259-72-3,10060-40-9,111-78-4
cyclo-octa-1,5-diene

: 351203-69-5
[chloro-η4-(1,5-cyclooctadiene)-κ-P-(1-(diphenyl(2-diphenylphosphinoethyl)phosphonio)-3-triphenylphosphoniobenzo[c]phospholide)rhodium(I)]Tetraphenylborate

Guidance literature:: In tetrahydrofuran; dichloromethane; under dry Ar; the ligand was added to a suspn. of Rh complex in THF and CH2Cl2, the mixt. was stirred for 15 h; concd. in vac., hexane was added, ppt. was filtered, washed with hexane,dried in vac.; elem. anal.;

Reference yield:

: 12092-47-6
di-μ-chloro-bis(1,5-cyclooctadiene)dirhodium

: 351203-64-0
[1-[(2-diphenylphosphinoethyl)-diphenylphosphonio]-3-triphenylphosphonio-benzo[c]phospholide] tetraphenylborate

: 5259-72-3,10060-40-9,111-78-4
cyclo-octa-1,5-diene

: 351203-69-5
[chloro-η4-(1,5-cyclooctadiene)-κ-P-(1-(diphenyl(2-diphenylphosphinoethyl)phosphonio)-3-triphenylphosphoniobenzo[c]phospholide)rhodium(I)]Tetraphenylborate

Guidance literature:: In tetrahydrofuran; under dry Ar; cyclooctadiene was added to a soln. of Rh complex and tetraphenylborate in THF, the mixt. was stirred for 5 h; (CH3CH2)2O and hexane was added, ppt. was filtered, washed with hexane, dried in vac.; elem. anal.;