C₁₈H₂₂N₂O₃

Base Information

Chemical Name:C₁₈H₂₂N₂O₃
CAS No.:1113001-69-6
Molecular Formula:C₁₈H₂₂N₂O₃
Molecular Weight:314.384
Hs Code.:

C<sub>18</sub>H<sub>22</sub>N<sub>2</sub>O<sub>3</sub>

Synonyms:

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Chemical Property of C₁₈H₂₂N₂O₃

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Technology Process of C₁₈H₂₂N₂O₃

There total 7 articles about C₁₈H₂₂N₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 83249-10-9
3‐(methoxycarbonyl)bicyclo[1.1.1]pentane‐1‐carboxylic acid

: 1113001-69-6
C₁₈H₂₂N₂O₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: chloroformic acid ethyl ester; triethylamine / tetrahydrofuran / 0.5 h / -15 °C / Inert atmosphere

1.2: 24.5 h / -4 - 0 °C

1.3: 0.5 h / 20 °C / Sonication

2.1: borane-THF / tetrahydrofuran / 6 h / -15 °C

3.1: Dess-Martin periodane / dichloromethane / 1 h / 0 °C

4.1: methanol / 8 h / 20 °C

5.1: methanol / 24 h / 0 - 20 °C

With methanol; borane-THF; chloroformic acid ethyl ester; Dess-Martin periodane; triethylamine; In tetrahydrofuran; methanol; dichloromethane; 1.1: Arndt-Eistert synthesis / 1.2: Arndt-Eistert synthesis / 1.3: Arndt-Eistert synthesis / 3.1: Dess-Martin oxidation;
DOI:10.1016/j.bmc.2008.11.015

Reference yield:

: 1113001-61-8
C₉H₁₀N₂O₃

: 1113001-69-6
C₁₈H₂₂N₂O₃

Guidance literature:: Multi-step reaction with 5 steps

1: water; silver benzoate; triethylamine / tetrahydrofuran / 0.5 h / 20 °C / Sonication

2: borane-THF / tetrahydrofuran / 6 h / -15 °C

3: Dess-Martin periodane / dichloromethane / 1 h / 0 °C

4: methanol / 8 h / 20 °C

5: methanol / 24 h / 0 - 20 °C

With methanol; borane-THF; water; silver benzoate; Dess-Martin periodane; triethylamine; In tetrahydrofuran; methanol; dichloromethane; 1: Wolff rearrangement / 3: Dess-Martin oxidation;
DOI:10.1016/j.bmc.2008.11.015

Reference yield:

: 1113001-63-0
2-(3-methoxycarbonylbicyclo[1.1.1]pentane)acetic acid

: 1113001-69-6
C₁₈H₂₂N₂O₃

Guidance literature:: Multi-step reaction with 4 steps

1: borane-THF / tetrahydrofuran / 6 h / -15 °C

2: Dess-Martin periodane / dichloromethane / 1 h / 0 °C

3: methanol / 8 h / 20 °C

4: methanol / 24 h / 0 - 20 °C

With methanol; borane-THF; Dess-Martin periodane; In tetrahydrofuran; methanol; dichloromethane; 2: Dess-Martin oxidation;
DOI:10.1016/j.bmc.2008.11.015