4-ethylthio-4'-ferrocenylbiphenyl

Base Information

Chemical Name:4-ethylthio-4'-ferrocenylbiphenyl
CAS No.:661466-14-4
Molecular Formula:C₂₄H₂₂FeS
Molecular Weight:398.352
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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-ethylthio-4'-ferrocenylbiphenyl

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Technology Process of 4-ethylthio-4'-ferrocenylbiphenyl

There total 1 articles about 4-ethylthio-4'-ferrocenylbiphenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 284688-05-7
1-(4'-bromobiphenyl-4-yl)-ferrocene

: 811-51-8
sodium thioethylate

: 661466-14-4
4-ethylthio-4'-ferrocenylbiphenyl

Guidance literature:: With aq. HCl; In further solvent(s); Ar; addn. of sodium ethylthiolate and anhyd. hexamethylphosphoramide to the complex, stirring at 95°C for 2.5 h, cooling to 20°C, pouring into a mixt. of 36% HCl and water; extn. of the organic phase with ether, sepn., drying the organic layer with MgSO4, filtration, ether removal in vac., chromy. (aluminum oxide, 1:4 benzene-light petroleum, recrystn. from. light petroleum; elem. anal.;
DOI:10.1023/A:1023998420937