ferrocenyl-2,4,6-triisopropylphenyldibromogermane

Base Information

Chemical Name:ferrocenyl-2,4,6-triisopropylphenyldibromogermane
CAS No.:1375102-13-8
Molecular Formula:C₂₅H₃₂Br₂FeGe
Molecular Weight:620.774
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ferrocenyl-2,4,6-triisopropylphenyldibromogermane

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Technology Process of ferrocenyl-2,4,6-triisopropylphenyldibromogermane

There total 1 articles about ferrocenyl-2,4,6-triisopropylphenyldibromogermane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 558-13-4
carbon tetrabromide

: 1375102-12-7
ferrocenyl-2,4,6-triisopropylphenylgermane

: 1375102-13-8
ferrocenyl-2,4,6-triisopropylphenyldibromogermane

Guidance literature:: In benzene; (Ar); refluxed for 1 h; cooled to ambient temp., evapd. (vac.), extd. (hexane), filtered, evapd.(vac.), chromd. (GPLC, toluene); elem. anal.;
DOI:10.1021/om300064q

Reference yield: 51.0%

: 1375102-13-8
ferrocenyl-2,4,6-triisopropylphenyldibromogermane

: 1375102-11-6
(E)-1,2-bis(ferrocenyl)-1,2-bis(2,4,6-triisopropylphenyl)digermene

Guidance literature:: With KC₈; In tetrahydrofuran; (Ar); KC8 added to a soln. of Fe complex at -78°C, stirred at -78°C for 1 h, warmed to -50°C and stirred for 30 min at thistemp.; evapd. (vac., at room temp.), taken up in hexane, filtered, evapd. (vac.), recrystd. (hexane);
DOI:10.1021/om300064q