Technology Process of C35H29NO10
There total 1 articles about C35H29NO10 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: H2; triethylamine / Pd/C / diethyl ether; hexane / 3 h
2: 3.06 g / diethyl ether; hexane / 10 h / 20 °C
With
hydrogen; triethylamine;
palladium on activated charcoal;
In
diethyl ether; hexane;
DOI:10.1002/ejoc.200300483
- Guidance literature:
-
Multi-step reaction with 4 steps
1: PPh3; CBr4; triethylamine / CH2Cl2 / 0.5 h / -20 °C
2: pyridine N-oxide; molecular sieves (3 Angstroem); iodine / acetonitrile / 0.17 h
3: 356 mg / acetonitrile / 0.5 h
4: H2 / Pd/C / methanol / 10 h
With
pyridine N-oxide; carbon tetrabromide; 3 A molecular sieve; hydrogen; iodine; triethylamine; triphenylphosphine;
palladium on activated charcoal;
In
methanol; dichloromethane; acetonitrile;
DOI:10.1002/ejoc.200300483
- Guidance literature:
-
Multi-step reaction with 4 steps
1: PPh3; CBr4; triethylamine / CH2Cl2 / 0.5 h / -20 °C
2: pyridine N-oxide; molecular sieves (3 Angstroem); iodine / acetonitrile / 0.17 h
3: 387 mg / acetonitrile / 0.5 h
4: H2 / Pd/C / methanol / 18 h
With
pyridine N-oxide; carbon tetrabromide; 3 A molecular sieve; hydrogen; iodine; triethylamine; triphenylphosphine;
palladium on activated charcoal;
In
methanol; dichloromethane; acetonitrile;
DOI:10.1002/ejoc.200300483
