Technology Process of C24H32INO4S
There total 3 articles about C24H32INO4S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: copper(l) iodide / diethyl ether / 18 h / -78 - 20 °C / Inert atmosphere
1.2: 1 h / -78 - 20 °C
1.3: 0 °C / Saturated gas
2.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 20 °C
3.1: potassium carbonate / acetone / Reflux
With
copper(l) iodide; di-isopropyl azodicarboxylate; potassium carbonate; triphenylphosphine;
In
tetrahydrofuran; diethyl ether; acetone;
2.1: Mitsunobu reaction;
DOI:10.1039/c1cc15257b
- Guidance literature:
-
Multi-step reaction with 2 steps
1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 20 °C
2: potassium carbonate / acetone / Reflux
With
di-isopropyl azodicarboxylate; potassium carbonate; triphenylphosphine;
In
tetrahydrofuran; acetone;
1: Mitsunobu reaction;
DOI:10.1039/c1cc15257b