(η5-cyclopentadienyl)(1,10-phenanthroline)(η1-1,5-bis(diphenylphosphino)pentane)ruthenium(II) hexafluorophosphate

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Chemical Name:(η5-cyclopentadienyl)(1,10-phenanthroline)(η1-1,5-bis(diphenylphosphino)pentane)ruthenium(II) hexafluorophosphate
CAS No.:108970-60-1
Molecular Formula:C₄₆H₄₃N₂P₂Ru*F₆P
Molecular Weight:931.843
Hs Code.:

Synonyms:

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Chemical Property of (η5-cyclopentadienyl)(1,10-phenanthroline)(η1-1,5-bis(diphenylphosphino)pentane)ruthenium(II) hexafluorophosphate

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Technology Process of (η5-cyclopentadienyl)(1,10-phenanthroline)(η1-1,5-bis(diphenylphosphino)pentane)ruthenium(II) hexafluorophosphate

There total 1 articles about (η5-cyclopentadienyl)(1,10-phenanthroline)(η1-1,5-bis(diphenylphosphino)pentane)ruthenium(II) hexafluorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: ammonium hexafluorophosphate

: chloro(η5-cyclopentadienyl)(1,10-phenanthroline)ruthenium(II)

: 27721-02-4
1,5-bis-(diphenylphosphino)pentane

: 108970-60-1
(η5-cyclopentadienyl)(1,10-phenanthroline)(η1-1,5-bis(diphenylphosphino)pentane)ruthenium(II) hexafluorophosphate

Guidance literature:: In ethanol; a suspn. of Ru-complex in EtOH at 0°C was treated with a soln. of the diphosphine (1:1 mole ratio) in EtOH under inert atmosphere, mixt. was stirred at 0°C for 1 h, filtered, concd., an ethanolic soln. of NH4PF6 was added with stirring; ppt. was isolated by filtration and washed with diethyl ether; elem. anal.;

Reference yield: 90.0%

: ammonium hexafluorophosphate

: 93966-27-9
(η5-cyclopentadienyl)(2,2'-bipyridine)ruthenium(II) chloride

: 108970-60-1
(η5-cyclopentadienyl)(1,10-phenanthroline)(η1-1,5-bis(diphenylphosphino)pentane)ruthenium(II) hexafluorophosphate

: 108970-64-5
bis(η5-cyclopentadienyl)(1,10-phenanthroline)(2,2'-bipyridine)(μ-1,5-bis(diphenylphosphino)pentane)diruthenium(II) hexafluorophosphate

Guidance literature:: In ethanol; a suspn. of both Ru-complexes in ethanol was heated under reflux for 20 min under inert atmosphere; cooled to room temp., ppt. was collected by filtration and washed with Et2O, treatment of the filtrate with NH4PF6 in EtOH with stirring afforded a second crop of the binuclear complex; elem. anal.;