Technology Process of C14H20O2
There total 3 articles about C14H20O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: triethylamine / dichloromethane / 0.33 h / 20 °C / Molecular sieve; Inert atmosphere
1.2: 5 h / 20 °C / Inert atmosphere
2.1: potassium carbonate; (1,2-dimethoxyethane)dichloronickel(II); 4,4'-dimethyl-2,2'-bipyridines / acetonitrile / 24 h / 70 °C / Inert atmosphere; Glovebox; Molecular sieve
With
4,4'-dimethyl-2,2'-bipyridines; (1,2-dimethoxyethane)dichloronickel(II); potassium carbonate; triethylamine;
In
dichloromethane; acetonitrile;
2.1: |Suzuki-Miyaura Coupling;
DOI:10.1021/acs.orglett.9b02643
- Guidance literature:
-
With
4,4'-dimethyl-2,2'-bipyridines; (1,2-dimethoxyethane)dichloronickel(II); potassium carbonate;
In
acetonitrile;
at 70 ℃;
for 24h;
Reagent/catalyst;
Solvent;
Catalytic behavior;
Inert atmosphere;
Glovebox;
Molecular sieve;
DOI:10.1021/acs.orglett.9b02643
- Guidance literature:
-
With
4,4'-dimethyl-2,2'-bipyridines; (1,2-dimethoxyethane)dichloronickel(II); potassium carbonate;
In
acetonitrile;
at 70 ℃;
for 24h;
Temperature;
Catalytic behavior;
Inert atmosphere;
Sealed tube;
DOI:10.1021/acs.orglett.9b02643
