anti,anti,syn-trishomocycloheptatrienyl 3,5-dinitrobenzoate

Base Information

Chemical Name:anti,anti,syn-trishomocycloheptatrienyl 3,5-dinitrobenzoate
CAS No.:73594-15-7
Molecular Formula:C₁₇H₁₆N₂O₆
Molecular Weight:344.324
Hs Code.:

Synonyms:

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Chemical Property of anti,anti,syn-trishomocycloheptatrienyl 3,5-dinitrobenzoate

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Technology Process of anti,anti,syn-trishomocycloheptatrienyl 3,5-dinitrobenzoate

There total 26 articles about anti,anti,syn-trishomocycloheptatrienyl 3,5-dinitrobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 73594-15-7,73611-22-0,73611-23-1,73611-24-2
syn,anti,anti-trishomocycloheptatrienyl 3,5-dinitrobenzoate

: 73594-19-1,73611-28-6,73611-30-0,73611-32-2
anti,anti,anti-trishomocycloheptatrienol

: 73594-19-1,73611-28-6,73611-30-0,73611-32-2
C₁₀H₁₄O

: 73594-15-7,73611-22-0,73611-23-1,73611-24-2
C₁₇H₁₆N₂O₆

Guidance literature:: With 2,6-dimethylpyridine; In water; acetone; at 60 ℃; for 4h;
DOI:10.1021/ja00523a027

Reference yield:

: 67229-09-8,68128-36-9
anti-2,4-bishomotropone

: 73594-15-7,73611-22-0,73611-23-1,73611-24-2
C₁₇H₁₆N₂O₆

Guidance literature:: Multi-step reaction with 3 steps

1: 35 percent / sodium hydride / dimethylsulfoxide; tetrahydrofuran / 1.) room temperature, 1 h, 2.) 0 - 5 deg C, 1 h; room temperature, 2 h, 40 - 45 deg C, 10 min

2: diisobutylaluminum hydride / diethyl ether; heptane / 1.) -78 deg C, 2 h, 2.) room temperature, 1 h

3: pyridine

With sodium hydride; diisobutylaluminium hydride; In tetrahydrofuran; pyridine; diethyl ether; n-heptane; dimethyl sulfoxide;
DOI:10.1021/ja00523a027

Reference yield:

: 73594-19-1,73611-28-6,73611-30-0,73611-32-2
anti,anti,anti-trishomocycloheptatrienol

: 73594-15-7,73611-22-0,73611-23-1,73611-24-2
C₁₇H₁₆N₂O₆

Guidance literature:: Multi-step reaction with 3 steps

1: 41 percent / MnO₂ / cyclohexane / 24 h / Heating

2: diisobutylaluminum hydride / diethyl ether; heptane / 1.) -78 deg C, 2 h, 2.) room temperature, 1 h

3: pyridine

With manganese(IV) oxide; diisobutylaluminium hydride; In pyridine; diethyl ether; n-heptane; cyclohexane;
DOI:10.1021/ja00523a027