Technology Process of C24H28N8O2
There total 9 articles about C24H28N8O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
N-ethyl-N,N-diisopropylamine;
In
N,N-dimethyl-formamide;
at 120 ℃;
for 0.25h;
Microwave irradiation;
DOI:10.1021/jm301389h
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: trifluoroacetic acid / dichloromethane / 20 °C
1.2: tetraalkylammonium carbonate polymer-bound resin / 20 °C / pH > 7
2.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.25 h / 120 °C / Microwave irradiation
With
N-ethyl-N,N-diisopropylamine; trifluoroacetic acid;
In
dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm301389h
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: tetraalkylammonium carbonate polymer-bound resin / dichloromethane / 1 h / 20 °C
2.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C
3.1: tetrakis(triphenylphosphine) palladium(0); potassium acetate; sodium carbonate / water; acetonitrile / 120 °C / Microwave irradiation
4.1: trifluoroacetic acid / dichloromethane / 20 °C
4.2: tetraalkylammonium carbonate polymer-bound resin / 20 °C / pH > 7
5.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.25 h / 120 °C / Microwave irradiation
With
tetrakis(triphenylphosphine) palladium(0); potassium acetate; sodium carbonate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid;
In
dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
3.1: |Suzuki Coupling;
DOI:10.1021/jm301389h
