Cbz-Phe-Glyψ-(R,S)Ala-OH

Base Information

Chemical Name:Cbz-Phe-Glyψ-(R,S)Ala-OH
CAS No.:137862-12-5
Molecular Formula:C₂₃H₂₆N₂O₅
Molecular Weight:410.47
Hs Code.:

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Chemical Property of Cbz-Phe-Glyψ-(R,S)Ala-OH

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Technology Process of Cbz-Phe-Glyψ-(R,S)Ala-OH

There total 5 articles about Cbz-Phe-Glyψ-(R,S)Ala-OH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 144422-93-5,144422-99-1
E-1-amino(Cbz-Phe)-4-methyl-2-penten-5-ol

: 137862-12-5,137862-13-6
Cbz-Phe-Glyψ-(R,S)Ala-OH

Guidance literature:: With jones' reagent; In acetone; 1.) 0.5 h, 0 deg C, 2.) 3.5 h r.t.;
DOI:10.1016/S0040-4020(01)88232-6

Reference yield:

: 1161-13-3
N-Cbz-L-Phe

: 137862-12-5,137862-13-6
Cbz-Phe-Glyψ-(R,S)Ala-OH

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) Et₃N, N-methylmorpholine, 2.) isobutylchloroformate / 1.) THF, DMF; 2.) DMF, 2 h, r.t.

2: 35 percent / Jones' reagent / acetone / 1.) 0.5 h, 0 deg C, 2.) 3.5 h r.t.

With 4-methyl-morpholine; jones' reagent; triethylamine; isobutyl chloroformate; In acetone;
DOI:10.1016/S0040-4020(01)88232-6

Reference yield:

: 137862-11-4
(E)-5-Amino-2-methyl-pent-3-en-1-ol

: 137862-12-5,137862-13-6
Cbz-Phe-Glyψ-(R,S)Ala-OH

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) Et₃N, N-methylmorpholine, 2.) isobutylchloroformate / 1.) THF, DMF; 2.) DMF, 2 h, r.t.

2: 35 percent / Jones' reagent / acetone / 1.) 0.5 h, 0 deg C, 2.) 3.5 h r.t.

With 4-methyl-morpholine; jones' reagent; triethylamine; isobutyl chloroformate; In acetone;
DOI:10.1016/S0040-4020(01)88232-6