ReCl(N₂)(NCC₆H₅)(P(OCH₃)3)3

Base Information

Chemical Name:ReCl(N₂)(NCC₆H₅)(P(OCH₃)3)3
CAS No.:152465-94-6
Molecular Formula:C₁₆H₃₂ClN₃O₉P₃Re
Molecular Weight:725.026
Hs Code.:

ReCl(N<sub>2</sub>)(NCC<sub>6</sub>H<sub>5</sub>)(P(OCH<sub>3</sub>)3)3

Synonyms:

Suppliers and Price of ReCl(N₂)(NCC₆H₅)(P(OCH₃)3)3

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of ReCl(N₂)(NCC₆H₅)(P(OCH₃)3)3

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of ReCl(N₂)(NCC₆H₅)(P(OCH₃)3)3

There total 2 articles about ReCl(N₂)(NCC₆H₅)(P(OCH₃)3)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 152391-88-3,77690-14-3
dichloro(benzoyldiazenido)(trimethylphosphite)3rhenium

: 100-47-0
benzonitrile

: 152465-94-6
ReCl(N₂)(NCC₆H₅)(P(OCH₃)3)3

Guidance literature:: With sodium methylate; In dichloromethane; byproducts: NaCl, PhCOOMe; soln. of Re-complex in CH2Cl2 is refluxed (under N2) together with PhCN in the presence of NaOMe for 2 h; evapn. of solvent, washing with diethyl ether, recrystn. from THF/Et2O, elem. anal.;
DOI:10.1007/BF00817310

Reference yield:

: 124648-75-5,84605-44-7
ReClN₂(P(C₆H₅)3)(P(OCH₃)3)3

: 100-47-0
benzonitrile

: 152465-94-6
ReCl(N₂)(NCC₆H₅)(P(OCH₃)3)3

Guidance literature:: In tetrahydrofuran; byproducts: PPh3; replacement of PPh3 in the Re-compd. by PhCN; reaction in THF (under N2);
DOI:10.1007/BF00817310