HCCo₃(CO)7(CH(P(C₆H₅)2)3)

Base Information

• Chemical Name: HCCo₃(CO)7(CH(P(C₆H₅)2)3)
• CAS No.: 90999-49-8
• Molecular Formula: C₄₅H₃₂Co₃O₇P₃
• Molecular Weight: 954.646
• Mol file: 90999-49-8.mol

Synonyms:

Chemical Property of HCCo₃(CO)7(CH(P(C₆H₅)2)3)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of HCCo₃(CO)7(CH(P(C₆H₅)2)3)

There total 1 articles about HCCo₃(CO)7(CH(P(C₆H₅)2)3) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methylidenetricobalt nonacarbonyl (15664-75-2) + Tris(diphenylphosphino)methan (28926-65-0) → HCCo3(CO)7(CH(P(C6H5)2)3) (90999-49-8)

Guidance literature:

In toluene; stirring at 25°C for 96 h, evapg., extn. with toluene, filtration; pptn. with heptane, recrystn. from toluene/heptane; elem. anal.;

DOI:10.1016/S0022-328X(00)99162-9

Reference yield: 30.0%

HCCo3(CO)7(CH(P(C6H5)2)3) (90999-49-8) → HCCo3(CO)6(CH(P(C6H5)2)3) (90999-51-2)

Guidance literature:

In toluene; heating at 70°C for 12 h, pptn. with heptane, ppt. was discarded, soln. evapn.; crystn. from CH2Cl2/heptane; elem. anal.;

DOI:10.1016/S0022-328X(00)99162-9

upstream raw materials:

methylidenetricobalt nonacarbonyl

Tris(diphenylphosphino)methan

Downstream raw materials:

HCCo₃(CO)6(CH(P(C₆H₅)2)3)