N-(4-nitrobenzene)sulfonyl sym-(2-naphthyl)dibenzo-16-crown-5-oxyacetamide

Base Information

Chemical Name:N-(4-nitrobenzene)sulfonyl sym-(2-naphthyl)dibenzo-16-crown-5-oxyacetamide
CAS No.:1233736-36-1
Molecular Formula:C₃₇H₃₄N₂O₁₁S
Molecular Weight:714.75
Hs Code.:

Synonyms:

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Chemical Property of N-(4-nitrobenzene)sulfonyl sym-(2-naphthyl)dibenzo-16-crown-5-oxyacetamide

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Technology Process of N-(4-nitrobenzene)sulfonyl sym-(2-naphthyl)dibenzo-16-crown-5-oxyacetamide

There total 6 articles about N-(4-nitrobenzene)sulfonyl sym-(2-naphthyl)dibenzo-16-crown-5-oxyacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 34813-49-5
t-butylsulfonamide

: 1233736-29-2
C₃₁H₂₉ClO₇

: 1233736-36-1
N-(4-nitrobenzene)sulfonyl sym-(2-naphthyl)dibenzo-16-crown-5-oxyacetamide

Guidance literature:: t-butylsulfonamide; With sodium hydride; In tetrahydrofuran; at 20 ℃; for 1.5h; Inert atmosphere;

C₃₁H₂₉ClO₇; In tetrahydrofuran; at 20 ℃;
DOI:10.3998/ark.5550190.0011.708

Reference yield:

: 6325-93-5
p-nitrobenzenesulfonamide

: 1233736-29-2
C₃₁H₂₉ClO₇

: 1233736-36-1
N-(4-nitrobenzene)sulfonyl sym-(2-naphthyl)dibenzo-16-crown-5-oxyacetamide

Guidance literature:: p-nitrobenzenesulfonamide; With sodium hydride; In tetrahydrofuran; at 20 ℃; for 1.5h; Inert atmosphere;

C₃₁H₂₉ClO₇; In tetrahydrofuran; at 20 ℃; for 3h;
DOI:10.3998/ark.5550190.0011.708

Reference yield:

: 81633-82-1
sym-(keto)dibenzo-16-crown-5

: 1233736-36-1
N-(4-nitrobenzene)sulfonyl sym-(2-naphthyl)dibenzo-16-crown-5-oxyacetamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: magnesium / tetrahydrofuran / 20 °C / Inert atmosphere; Heating

2.1: sodium hydride / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

3.1: oxalyl dichloride / benzene / 1.5 h / 20 °C

4.1: sodium hydride / tetrahydrofuran / 1.5 h / 20 °C / Inert atmosphere

4.2: 20 °C

With oxalyl dichloride; sodium hydride; magnesium; In tetrahydrofuran; benzene;
DOI:10.3998/ark.5550190.0011.708