Technology Process of 4-ethylthio-3,3-diphenyl-3,4-dihydroquinoline
There total 4 articles about 4-ethylthio-3,3-diphenyl-3,4-dihydroquinoline which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium hydroxide / dimethyl sulfoxide / 2.33 h / 20 °C
2: diethyl ether / 16 h / 20 °C / Inert atmosphere
3: o-xylene / 0.5 h / 20 °C / Inert atmosphere
4: o-xylene / 1 h / Inert atmosphere; Reflux
With
potassium hydroxide;
In
diethyl ether; o-xylene; dimethyl sulfoxide;
2: |Staudinger Azide Reduction / 3: |Aza-Wittig Reaction;
DOI:10.1039/c2ob27010b
- Guidance literature:
-
In
o-xylene;
for 1h;
Inert atmosphere;
Reflux;
DOI:10.1039/c2ob27010b
- Guidance literature:
-
Multi-step reaction with 3 steps
1: diethyl ether / 16 h / 20 °C / Inert atmosphere
2: o-xylene / 0.5 h / 20 °C / Inert atmosphere
3: o-xylene / 1 h / Inert atmosphere; Reflux
In
diethyl ether; o-xylene;
1: |Staudinger Azide Reduction / 2: |Aza-Wittig Reaction;
DOI:10.1039/c2ob27010b
