1-(2,3-dihydro-1H-inden-4-yl)-N-methylmethanamine

Base Information

Chemical Name:1-(2,3-dihydro-1H-inden-4-yl)-N-methylmethanamine
CAS No.:17450-61-2
Molecular Formula:C₁₁H₁₅N
Molecular Weight:161.247
Hs Code.:

Synonyms:

Suppliers and Price of 1-(2,3-dihydro-1H-inden-4-yl)-N-methylmethanamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 4 raw suppliers

Chemical Property of 1-(2,3-dihydro-1H-inden-4-yl)-N-methylmethanamine

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1-(2,3-dihydro-1H-inden-4-yl)-N-methylmethanamine

There total 6 articles about 1-(2,3-dihydro-1H-inden-4-yl)-N-methylmethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: tert-butyl ((2,3-dihydro-1H-inden-4-yl)methyl)carbamate

: 17450-61-2
1-(2,3-dihydro-1H-inden-4-yl)-N-methylmethanamine

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃; Inert atmosphere; Reflux;
DOI:10.1021/acs.jmedchem.6b00122

Reference yield:

: 1285718-21-9
4-iodo-2,3-dihydro-1H-indene

: 17450-61-2
1-(2,3-dihydro-1H-inden-4-yl)-N-methylmethanamine

Guidance literature:: Multi-step reaction with 4 steps

1: N,N-dimethyl-formamide / 130 °C

2: lithium aluminium tetrahydride / tetrahydrofuran / -78 - 20 °C / Inert atmosphere

3: sodium hydroxide / tetrahydrofuran / 1 h / 0 - 20 °C

4: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C / Inert atmosphere; Reflux

With lithium aluminium tetrahydride; sodium hydroxide; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/acs.jmedchem.6b00122

Reference yield:

: 15115-63-6
2,3-dihydro-1H-indene-4-carbonitrile

: 17450-61-2
1-(2,3-dihydro-1H-inden-4-yl)-N-methylmethanamine

Guidance literature:: Multi-step reaction with 3 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / -78 - 20 °C / Inert atmosphere

2: sodium hydroxide / tetrahydrofuran / 1 h / 0 - 20 °C

3: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C / Inert atmosphere; Reflux

With lithium aluminium tetrahydride; sodium hydroxide; In tetrahydrofuran;
DOI:10.1021/acs.jmedchem.6b00122