allylbenzylbis[2,4,6-triisopropylphenyl]tin(IV)

Base Information

Chemical Name:allylbenzylbis[2,4,6-triisopropylphenyl]tin(IV)
CAS No.:887127-45-9
Molecular Formula:C₄₀H₅₈Sn
Molecular Weight:657.611
Hs Code.:

Synonyms:

Suppliers and Price of allylbenzylbis[2,4,6-triisopropylphenyl]tin(IV)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of allylbenzylbis[2,4,6-triisopropylphenyl]tin(IV)

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of allylbenzylbis[2,4,6-triisopropylphenyl]tin(IV)

There total 3 articles about allylbenzylbis[2,4,6-triisopropylphenyl]tin(IV) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 887127-44-8
benzylbromobis[2,4,6-triisopropylphenyl]tin(IV)

: 1730-25-2
allylmagnesium bromide

: 887127-45-9
allylbenzylbis[2,4,6-triisopropylphenyl]tin(IV)

Guidance literature:: In tetrahydrofuran; toluene; (under N2, Schlenk); soln. of allylmagnesium bromide in THF added dropwise to stirred soln. of Sn-compound in toluene at 0°C, refluxed for 2 d; quenched with H2O, aq. soln. of HBr, washed with H2O, NaHCO3, H2O, driedover MgSO4, solvent removed, crystd. from MeOH/hexane at -20°C; elem. anal.;
DOI:10.1016/j.jorganchem.2005.12.011

Reference yield:

: 108894-99-1
(2,4,6-triisopropylphenyl)magnesium bromide

: 887127-45-9
allylbenzylbis[2,4,6-triisopropylphenyl]tin(IV)

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran

2: tetrahydrofuran; toluene

In tetrahydrofuran; toluene;
DOI:10.1016/j.jorganchem.2005.12.011

Reference yield:

: 1589-82-8
phenylmagnesium bromide

: 887127-45-9
allylbenzylbis[2,4,6-triisopropylphenyl]tin(IV)

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran

2: tetrahydrofuran; toluene

In tetrahydrofuran; toluene;
DOI:10.1016/j.jorganchem.2005.12.011