bis(vanillin)diethylenetriimine

Base Information

Chemical Name:bis(vanillin)diethylenetriimine
CAS No.:92559-72-3
Molecular Formula:C₂₀H₂₅N₃O₄
Molecular Weight:371.436
Hs Code.:

Synonyms:

Suppliers and Price of bis(vanillin)diethylenetriimine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis(vanillin)diethylenetriimine

Chemical Property:

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Technology Process of bis(vanillin)diethylenetriimine

There total 1 articles about bis(vanillin)diethylenetriimine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 121-33-5,8014-42-4
vanillin

: 111-40-0,98824-35-2
3-azapentane-1,5-diamine

: 92559-72-3
bis(vanillin)diethylenetriimine

Guidance literature:: In ethanol;

Reference yield: 80.0%

: nickel(II)(ethyl acetoacetate)2(H₂O)2

: 92559-72-3
bis(vanillin)diethylenetriimine

: [bis(ethylacetoacetato)(bis(vanillin)diethylenetriimine)] nickel(II)

Guidance literature:: In ethanol; benzene; benzene soln. of Ni-complex was added to ethanolic soln. of Schiff baseat room temp., reflux for 1h; volume of soln. was reduced to 1/3, left in desiccator for 3-4 d, washed with several times with ether, dried in vac., elem. anal.;

Reference yield:

: 13477-89-9
neodymium(III) chloride hexahydrate

: 92559-72-3
bis(vanillin)diethylenetriimine

: Nd⁽³⁺⁾*C₆H₃(O)(OCH₃)CHNC₂H₄NHC₂H₄NCHC₆H₃(O)(OCH₃)^(2-)*Cl^(1-)*3H₂O = Nd(C₆H₃O(OCH₃)CHNC₂H₄NHC₂H₄NCHC₆H₃O(OCH₃))Cl*3H₂O

Guidance literature:: In ethanol; M. Shameen Ansari and N. A. Ahmad, J. Inorg. Nucl. Chem. 38, 1232 (1976); refluxed for about 6 h; elem. anal.;
DOI:10.1016/0022-1902(81)80496-4