copper(I) diphenylphosphide

Base Information

• Chemical Name: copper(I) diphenylphosphide
• CAS No.: 46225-54-1
• Molecular Formula: C₁₂H₁₀CuP
• Molecular Weight: 248.731

Synonyms:

Chemical Property of copper(I) diphenylphosphide

Chemical Property:

Purity/Quality:

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Technology Process of copper(I) diphenylphosphide

There total 5 articles about copper(I) diphenylphosphide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

(Me3Si)2NCu(Ph2P-NPh-NPhH)2 → copper(I) diphenylphosphide (46225-54-1)

Guidance literature:

In toluene; byproducts: azobenzene, Ph2P-NPh-NPhH, (Me3Si)2NH; (Ar or vac.); at 80°C for 2 h; filtered, washed (toluene), dried (vac.); elem. anal.;

DOI:10.1016/j.jorganchem.2004.06.056

Reference yield: 60.0%

copper (12775-96-1,15158-11-9,15721-63-8,16941-75-6,17493-86-6,19498-52-3,20499-83-6,20499-84-7,20499-85-8,20499-86-9,20573-10-8,20573-11-9,21595-51-7,21595-52-8,22206-52-6,26445-28-3,28959-95-7,37362-93-9,39417-05-5,54603-16-6,54603-23-5,54603-32-6,54603-40-6,54603-48-4,54603-81-5,54603-89-3,56316-56-4,95985-91-4,122297-32-9,7440-50-8) + diphenylphosphane (829-85-6) → copper(I) diphenylphosphide (46225-54-1)

Guidance literature:

In acetonitrile; Electrolysis; under N2; the electrolysis was performed in a cell containing platin as cathode and copper as anode at 35 V and 20 mA for 4.4 h; electrolyte: tetraethylammonium perchlorate;; the solution phase was decanted off; the residue was triturated with toluene and the residue was collected and washed with acetonitrile toluene and pentane and dried in vacuo; elem. anal.;;

DOI:10.1039/DT9910000011

Reference yield:

(CuO-t-Bu)4 + diphenylphosphane (829-85-6) → copper(I) diphenylphosphide (46225-54-1)

Guidance literature:

In benzene; byproducts: t-BuOH; under N2, in a Schlenk flask, 1 mol Ph2PH added, solution stirred; filtered, elem. anal.;

upstream raw materials:

copper

diphenylphosphane

copper(I) tert-butoxide

Downstream raw materials:

Cu⁽¹⁺⁾*P(C₆H₅)2^(1-)*C₁₄H₁₂N₂ = [Cu(P(C₆H₅)2)(C₁₄H₁₂N₂)]

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