C₂₇H₃₇N₇O₃

Base Information

Chemical Name:C₂₇H₃₇N₇O₃
CAS No.:1395172-00-5
Molecular Formula:C₂₇H₃₇N₇O₃
Molecular Weight:507.636
Hs Code.:

C<sub>27</sub>H<sub>37</sub>N<sub>7</sub>O<sub>3</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₇H₃₇N₇O₃

Chemical Property:

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Technology Process of C₂₇H₃₇N₇O₃

There total 3 articles about C₂₇H₃₇N₇O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 581-00-0
2-Methyl-4-morpholin-4-ylphenylamine

: C₁₆H₂₄N₆O₂

: 1395172-00-5
C₂₇H₃₇N₇O₃

Guidance literature:: With palladium diacetate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; In toluene; at 80 - 100 ℃;
DOI:10.1016/j.bmcl.2012.04.131

Reference yield:

: 220679-09-4
4-(3-methyl-4-nitrophenyl)morpholine

: 1395172-00-5
C₂₇H₃₇N₇O₃

Guidance literature:: Multi-step reaction with 2 steps

1: palladium 10% on activated carbon; hydrogen / methanol

2: palladium diacetate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / toluene / 80 - 100 °C

With palladium 10% on activated carbon; hydrogen; palladium diacetate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; In methanol; toluene; 2: Buchwald coupling;
DOI:10.1016/j.bmcl.2012.04.131

Reference yield:

: 5451-40-1
2,6 dichloropurine

: 1395172-00-5
C₂₇H₃₇N₇O₃

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / ethanol / 80 °C

2: toluene-4-sulfonic acid / tetrahydrofuran / Reflux

3: palladium diacetate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / toluene / 80 - 100 °C

With palladium diacetate; caesium carbonate; toluene-4-sulfonic acid; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; triethylamine; In tetrahydrofuran; ethanol; toluene; 3: Buchwald coupling;
DOI:10.1016/j.bmcl.2012.04.131