15,18-dimethyl-14,19-diphenyl-3,11,22,30,36,37,38-heptaazahexacyclo[30.3.1.1(3,16).1(17,20).0(5,19).0(23,28)]octatriaconta-1⁽³⁶⁾,5⁽¹⁰⁾,6,8,13,15,17,19,23,25,27,32,34-tridecaene-2,12,21,31-tetrone

Base Information

• Chemical Name: 15,18-dimethyl-14,19-diphenyl-3,11,22,30,36,37,38-heptaazahexacyclo[30.3.1.1(3,16).1(17,20).0(5,19).0(23,28)]octatriaconta-1⁽³⁶⁾,5⁽¹⁰⁾,6,8,13,15,17,19,23,25,27,32,34-tridecaene-2,12,21,31-tetrone
• CAS No.: 1429988-61-3
• Molecular Formula: C₄₅H₃₇N₇O₄
• Molecular Weight: 739.833

Synonyms:

Chemical Property of 15,18-dimethyl-14,19-diphenyl-3,11,22,30,36,37,38-heptaazahexacyclo[30.3.1.1(3,16).1(17,20).0(5,19).0(23,28)]octatriaconta-1⁽³⁶⁾,5⁽¹⁰⁾,6,8,13,15,17,19,23,25,27,32,34-tridecaene-2,12,21,31-tetrone

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Technology Process of 15,18-dimethyl-14,19-diphenyl-3,11,22,30,36,37,38-heptaazahexacyclo[30.3.1.1(3,16).1(17,20).0(5,19).0(23,28)]octatriaconta-1⁽³⁶⁾,5⁽¹⁰⁾,6,8,13,15,17,19,23,25,27,32,34-tridecaene-2,12,21,31-tetrone

There total 4 articles about 15,18-dimethyl-14,19-diphenyl-3,11,22,30,36,37,38-heptaazahexacyclo[30.3.1.1(3,16).1(17,20).0(5,19).0(23,28)]octatriaconta-1⁽³⁶⁾,5⁽¹⁰⁾,6,8,13,15,17,19,23,25,27,32,34-tridecaene-2,12,21,31-tetrone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

2,6-Pyridinedicarbonyl dichloride (3739-94-4) + N5,N5'-bis(2-(aminomethyl)phenyl)-3,3'-dimethyl-4,4'-diphenyl-1H,1'H-[2,2'-bipyrrole]-5,5'-dicarboxamide (1429988-57-7) → 15,18-dimethyl-14,19-diphenyl-3,11,22,30,36,37,38-heptaazahexacyclo[30.3.1.1(3,16).1(17,20).0(5,19).0(23,28)]octatriaconta-1(36),5(10),6,8,13,15,17,19,23,25,27,32,34-tridecaene-2,12,21,31-tetrone (1429988-61-3)

Guidance literature:

With dmap; triethylamine; In tetrahydrofuran; for 12h;

DOI:10.1002/chem.201204306

Reference yield:

5-(5-carboxy-3-methyl-4-phenyl-1H-pyrrol-2-yl)-4-methyl-3-phenyl-1H-pyrrole-2-carboxylic acid (1013935-37-9) → 15,18-dimethyl-14,19-diphenyl-3,11,22,30,36,37,38-heptaazahexacyclo[30.3.1.1(3,16).1(17,20).0(5,19).0(23,28)]octatriaconta-1(36),5(10),6,8,13,15,17,19,23,25,27,32,34-tridecaene-2,12,21,31-tetrone (1429988-61-3)

Guidance literature:

Multi-step reaction with 4 steps

1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 20 °C / Inert atmosphere

2: tetrahydrofuran / 10 h / Inert atmosphere

3: trifluoroacetic acid / dichloromethane / 2 h

4: dmap; triethylamine / tetrahydrofuran / 12 h

With dmap; oxalyl dichloride; triethylamine; N,N-dimethyl-formamide; trifluoroacetic acid; In tetrahydrofuran; dichloromethane;

DOI:10.1002/chem.201204306

Reference yield:

3,3'-dimethyl-4,4'-diphenyl-1H,1'H-[2,2'-bipyrrole]-5,5'-dicarboxylic acid chloride (1092556-36-9) → 15,18-dimethyl-14,19-diphenyl-3,11,22,30,36,37,38-heptaazahexacyclo[30.3.1.1(3,16).1(17,20).0(5,19).0(23,28)]octatriaconta-1(36),5(10),6,8,13,15,17,19,23,25,27,32,34-tridecaene-2,12,21,31-tetrone (1429988-61-3)

Guidance literature:

Multi-step reaction with 3 steps

1: tetrahydrofuran / 10 h / Inert atmosphere

2: trifluoroacetic acid / dichloromethane / 2 h

3: dmap; triethylamine / tetrahydrofuran / 12 h

With dmap; triethylamine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane;

DOI:10.1002/chem.201204306

upstream raw materials:

2,6-Pyridinedicarbonyl dichloride

N₅,N₅'-bis(2-(aminomethyl)phenyl)-3,3'-dimethyl-4,4'-diphenyl-1H,1'H-[2,2'-bipyrrole]-5,5'-dicarboxamide

5-(5-carboxy-3-methyl-4-phenyl-1H-pyrrol-2-yl)-4-methyl-3-phenyl-1H-pyrrole-2-carboxylic acid

3,3'-dimethyl-4,4'-diphenyl-1H,1'H-[2,2'-bipyrrole]-5,5'-dicarboxylic acid chloride

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