3,3'-dimethyl-4,4'-diphenyl-1H,1'H-[2,2'-bipyrrole]-5,5'-dicarboxylic acid chloride

Base Information

• Chemical Name: 3,3'-dimethyl-4,4'-diphenyl-1H,1'H-[2,2'-bipyrrole]-5,5'-dicarboxylic acid chloride
• CAS No.: 1092556-36-9
• Molecular Formula: C₂₄H₁₈Cl₂N₂O₂
• Molecular Weight: 437.325

Synonyms:3,3'-dimethyl-4,4'-diphenyl-1H,1'H-[2,2'-bipyrrole]-5,5'-dicarboxylic acid chloride

Chemical Property of 3,3'-dimethyl-4,4'-diphenyl-1H,1'H-[2,2'-bipyrrole]-5,5'-dicarboxylic acid chloride

Chemical Property:

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Technology Process of 3,3'-dimethyl-4,4'-diphenyl-1H,1'H-[2,2'-bipyrrole]-5,5'-dicarboxylic acid chloride

There total 2 articles about 3,3'-dimethyl-4,4'-diphenyl-1H,1'H-[2,2'-bipyrrole]-5,5'-dicarboxylic acid chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-(5-carboxy-3-methyl-4-phenyl-1H-pyrrol-2-yl)-4-methyl-3-phenyl-1H-pyrrole-2-carboxylic acid (1013935-37-9) → 3,3'-dimethyl-4,4'-diphenyl-1H,1'H-[2,2'-bipyrrole]-5,5'-dicarboxylic acid chloride (1092556-36-9)

Guidance literature:

With oxalyl dichloride;

DOI:10.1002/chem.200800860

Reference yield:

oxalyl dichloride (79-37-8) + 3,3'-dimethyl-4,4'-diphenyl-2,2'-bipyrrole → 3,3'-dimethyl-4,4'-diphenyl-1H,1'H-[2,2'-bipyrrole]-5,5'-dicarboxylic acid chloride (1092556-36-9)

Guidance literature:

With N,N-dimethyl-formamide; In dichloromethane; at 20 ℃; for 3.5h; Inert atmosphere;

DOI:10.1002/ejoc.201301867

Reference yield: 60.0%

3,3'-dimethyl-4,4'-diphenyl-1H,1'H-[2,2'-bipyrrole]-5,5'-dicarboxylic acid chloride (1092556-36-9) + 1-(2-aminobenzyl)-2,3-di[(tert-butoxy)carbonyl]guanidine (1612875-10-1) → C60H72N10O10 (1612875-06-5)

Guidance literature:

With pyridine; dmap; In dichloromethane; at 20 ℃; for 48h; Inert atmosphere;

DOI:10.1002/ejoc.201301867

upstream raw materials:

5-(5-carboxy-3-methyl-4-phenyl-1H-pyrrol-2-yl)-4-methyl-3-phenyl-1H-pyrrole-2-carboxylic acid

oxalyl dichloride

Downstream raw materials:

C₄₄H₃₇N₇O₄

C₆₀H₄₈N₈O₄

N₅,N₅'-bis(2-(aminomethyl)phenyl)-3,3'-dimethyl-4,4'-diphenyl-1H,1'H-[2,2'-bipyrrole]-5,5'-dicarboxamide

15,18-dimethyl-14,19-diphenyl-3,11,22,30,36,37,38-heptaazahexacyclo[30.3.1.1(3,16).1(17,20).0(5,19).0(23,28)]octatriaconta-1⁽³⁶⁾,5⁽¹⁰⁾,6,8,13,15,17,19,23,25,27,32,34-tridecaene-2,12,21,31-tetrone

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