(1R,2S,3S,4S)-(3-phenylsulfonylaminobicyclo<2.2.1>hept-2-yl)pentamidoethylsulfonic acid

Base Information

Chemical Name:(1R,2S,3S,4S)-(3-phenylsulfonylaminobicyclo<2.2.1>hept-2-yl)pentamidoethylsulfonic acid
CAS No.:139434-95-0
Molecular Formula:C₂₀H₃₀N₂O₆S₂
Molecular Weight:458.6
Hs Code.:

Synonyms:

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Chemical Property of (1R,2S,3S,4S)-(3-phenylsulfonylaminobicyclo<2.2.1>hept-2-yl)pentamidoethylsulfonic acid

Chemical Property:

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Technology Process of (1R,2S,3S,4S)-(3-phenylsulfonylaminobicyclo<2.2.1>hept-2-yl)pentamidoethylsulfonic acid

There total 3 articles about (1R,2S,3S,4S)-(3-phenylsulfonylaminobicyclo<2.2.1>hept-2-yl)pentamidoethylsulfonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 128299-81-0
(3'R,4'R,5'S,6'S)-5'-(Formylmethyl)-4'-benzenesulfonamidobicyclo<2.2.1>heptane

: 139434-95-0
(1R,2S,3S,4S)-(3-phenylsulfonylaminobicyclo<2.2.1>hept-2-yl)pentamidoethylsulfonic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) tert-BuOK / 1.) THF, room temperature, 1 h, 2.) THF, -15 to 0 deg C, 1 h

2: 90 percent / H₂ / 10percent Pd/C / methanol / 0.33 h / Ambient temperature

3: 1.) DCC, HOSu, 2.) Et₃N / 1.) DMF, room temperature, 1.5 h, 2.) room temperature, overnight

With 1-hydroxy-pyrrolidine-2,5-dione; potassium tert-butylate; hydrogen; triethylamine; dicyclohexyl-carbodiimide; palladium on activated charcoal; In methanol;
DOI:10.1248/cpb.39.2842

Reference yield:

: 139559-71-0
Bisnor-(+)-S-145

: 139434-95-0
(1R,2S,3S,4S)-(3-phenylsulfonylaminobicyclo<2.2.1>hept-2-yl)pentamidoethylsulfonic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / H₂ / 10percent Pd/C / methanol / 0.33 h / Ambient temperature

2: 1.) DCC, HOSu, 2.) Et₃N / 1.) DMF, room temperature, 1.5 h, 2.) room temperature, overnight

With 1-hydroxy-pyrrolidine-2,5-dione; hydrogen; triethylamine; dicyclohexyl-carbodiimide; palladium on activated charcoal; In methanol;
DOI:10.1248/cpb.39.2842

Reference yield:

: 107-35-7
Tau

: 139559-72-1
(1R,2S,3S,4S)-5'-(3-phenylsulfonylaminobicyclo<2.2.1>hept-2-yl)pentanoic acid

: 139434-95-0
(1R,2S,3S,4S)-(3-phenylsulfonylaminobicyclo<2.2.1>hept-2-yl)pentamidoethylsulfonic acid

Guidance literature:: With 1-hydroxy-pyrrolidine-2,5-dione; triethylamine; dicyclohexyl-carbodiimide; Yield given. Multistep reaction; 1.) DMF, room temperature, 1.5 h, 2.) room temperature, overnight;
DOI:10.1248/cpb.39.2842